1-IODO-3,3,3-TRIFLUOROPROPANE

Base Information

• Chemical Name: 1-IODO-3,3,3-TRIFLUOROPROPANE
• CAS No.: 460-37-7
• Molecular Formula: C3H4F
• Molecular Weight: 223.964
• Hs Code.: 29037990
• European Community (EC) Number: 670-532-1
• DSSTox Substance ID: DTXSID10963475
• Nikkaji Number: J151.442C
• Wikidata: Q72484771
• Mol file: 460-37-7.mol

Synonyms:1,1,1-trifluoro-3-iodopropane;3,3,3-Trifluoro-1-iodopropane;3,3,3-Trifluoropropyl iodide;

Chemical Property of 1-IODO-3,3,3-TRIFLUOROPROPANE

Chemical Property:

• Appearance/Colour: Clear colorless to pink liquid
• Vapor Pressure: 64.9mmHg at 25°C
• Refractive Index: n20/D 1.42(lit.)
• Boiling Point: 89.9 °C at 760 mmHg
• Flash Point: 25.1 °C
• PSA: 0.00000
• Density: 1.977 g/cm³
• LogP: 2.37380
• Storage Temp.: 2-8°C(protect from light)
• Sensitive.: Light Sensitive
• XLogP3: 2.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 1
• Exact Mass: 223.93098
• Heavy Atom Count: 7
• Complexity: 48.6

Purity/Quality:

99% ^*data from raw suppliers

1,1,1-Trifluoro-3-iodopropane >98.0%(GC) ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36/37/39-24/25

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: C(CI)C(F)(F)F

Technology Process of 1-IODO-3,3,3-TRIFLUOROPROPANE

There total 8 articles about 1-IODO-3,3,3-TRIFLUOROPROPANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethene (74-85-1) + iodotrifluoromethane (2314-97-8,263005-66-9) → 1,1,1-trifluoro-3-iodopropane (460-37-7,71215-70-8) + vinyliodide (593-66-8) + 1,1,1-trifluoropropylene (677-21-4) + acetylene (74-86-2,25067-58-7)

Guidance literature:

under 820 Torr; Quantum yield; Irradiation; CO₂ laser induced telomerization;

DOI:10.1016/0584-8539(87)80083-1

Reference yield:

ethene (74-85-1) + iodotrifluoromethane (2314-97-8,263005-66-9) → 1,1,1-trifluoro-3-iodopropane (460-37-7,71215-70-8)

Guidance literature:

Irradiation_.mit UV-Licht;

Reference yield:

3-bromo-1,1,1-trifluoropropane (460-32-2) → 1,1,1-trifluoro-3-iodopropane (460-37-7,71215-70-8)

Guidance literature:

With acetone; sodium iodide;

DOI:10.1021/ja01167a069

upstream raw materials:

ethene

iodotrifluoromethane

3-bromo-1,1,1-trifluoropropane

3-iodopropanoic acid

Downstream raw materials:

3-chloro-1,1,1-trifluoropropane

1,1,1-trifluoropropylene

ethyl 4,4,4-trifluorobutanoate

4,4,4-trifluorobutyric acid

Refernces