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2-Bromo-5-iodo-3-methylpyridine

Base Information Edit
  • Chemical Name:2-Bromo-5-iodo-3-methylpyridine
  • CAS No.:65550-78-9
  • Molecular Formula:C6H5 Br I N
  • Molecular Weight:297.91900
  • Hs Code.:2933399090
  • European Community (EC) Number:678-919-7
  • DSSTox Substance ID:DTXSID40435791
  • Wikidata:Q72457556
  • Mol file:65550-78-9.mol
2-Bromo-5-iodo-3-methylpyridine

Synonyms:2-Bromo-5-iodo-3-methylpyridine;65550-78-9;2-Bromo-5-iodo-3-picoline;Pyridine, 2-bromo-5-iodo-3-methyl-;MFCD09037466;2-bromo-5-iodo-3-methyl-pyridine;SCHEMBL1929811;DTXSID40435791;WJPSANINUBHCFE-UHFFFAOYSA-N;AKOS015891658;DS-11870;SY041758;B4312;CS-0153175;FT-0646440;A21432;I10151;J-508385

Suppliers and Price of 2-Bromo-5-iodo-3-methylpyridine
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
  • TRC
  • 2-Bromo-5-iodo-3-methylpyridine
  • 500mg
  • $ 65.00
  • TRC
  • 2-Bromo-5-iodo-3-methylpyridine
  • 100mg
  • $ 45.00
  • TCI Chemical
  • 2-Bromo-5-iodo-3-methylpyridine >96.0%(GC)
  • 1g
  • $ 37.00
  • TCI Chemical
  • 2-Bromo-5-iodo-3-methylpyridine >96.0%(GC)
  • 5g
  • $ 182.00
  • SynQuest Laboratories
  • 2-Bromo-5-iodo-3-methylpyridine
  • 5 g
  • $ 228.00
  • SynQuest Laboratories
  • 2-Bromo-5-iodo-3-methylpyridine
  • 10 g
  • $ 364.00
  • Crysdot
  • 2-Bromo-5-iodo-3-methylpyridine 98%
  • 10g
  • $ 330.00
  • Crysdot
  • 2-Bromo-5-iodo-3-methylpyridine 98%
  • 5g
  • $ 220.00
  • Chemenu
  • 2-Bromo-5-iodo-3-methylpyridine 98%
  • 5g
  • $ 153.00
  • Chemenu
  • 2-Bromo-5-iodo-3-methylpyridine 98%
  • 10g
  • $ 224.00
Total 34 raw suppliers
Chemical Property of 2-Bromo-5-iodo-3-methylpyridine Edit
Chemical Property:
  • Vapor Pressure:0.002mmHg at 25°C 
  • Melting Point:43-46oC 
  • Boiling Point:298.047oC at 760 mmHg 
  • PKA:-0.94±0.20(Predicted) 
  • Flash Point:134.054oC 
  • PSA:12.89000 
  • Density:2.172g/cm3 
  • LogP:2.75710 
  • Storage Temp.:under inert gas (nitrogen or Argon) at 2–8 °C 
  • Sensitive.:Light Sensitive 
  • Solubility.:soluble in Methanol 
  • XLogP3:2.9
  • Hydrogen Bond Donor Count:0
  • Hydrogen Bond Acceptor Count:1
  • Rotatable Bond Count:0
  • Exact Mass:296.86501
  • Heavy Atom Count:9
  • Complexity:99.1
Purity/Quality:

97% *data from raw suppliers

2-Bromo-5-iodo-3-methylpyridine *data from reagent suppliers

Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
  • Statements: 22-36/37/38 
  • Safety Statements: 26-36/37 
MSDS Files:

SDS file from LookChem

Useful:
  • Canonical SMILES:CC1=CC(=CN=C1Br)I
Technology Process of 2-Bromo-5-iodo-3-methylpyridine

There total 4 articles about 2-Bromo-5-iodo-3-methylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With hydrogen bromide; bromine; sodium nitrite; at 0 ℃; for 0.5h;
DOI:10.1021/jo00121a071
Guidance literature:
2,5-dibromo-3-methylpyridine; With isopropylmagnesium chloride; In tetrahydrofuran; at 20 ℃; for 1h;
With iodine; In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1021/jm900450n
Guidance literature:
Multi-step reaction with 2 steps
1: 73 percent / HIO4*2H2O, I2, H2SO4 / aq. acetic acid / 4 h / 80 °C
2: 94 percent / 48percent HBr, Br2, aq. NaNO2 / 0.5 h / 0 °C
With sulfuric acid; hydrogen bromide; bromine; iodine; periodic acid; sodium nitrite; In acetic acid;
DOI:10.1021/jo00121a071
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