2,3-NAPHTHALENEDICARBOXIMIDE

Base Information

• Chemical Name: 2,3-NAPHTHALENEDICARBOXIMIDE
• CAS No.: 4379-54-8
• Molecular Formula: C12H7NO2
• Molecular Weight: 197.193
• Hs Code.: 2925190090
• Mol file: 4379-54-8.mol

Synonyms:2,3-Naphthalenedicarboximide(6CI,8CI);1,3-bb-Isonaphthazoledione;2,3-Naphthalimide;Benzo[f]isoindole-1,3-dione;NSC 343623;Naphthalene-2,3-dicarboxylic acid imide;Naphtho[2,3-c]pyrrole-1,3(2H)-dione;

Chemical Property of 2,3-NAPHTHALENEDICARBOXIMIDE

Chemical Property:

• Melting Point: 273-276 °C(lit.)
• Refractive Index: 1.708
• PSA: 46.17000
• Density: 1.391 g/cm³
• LogP: 2.05220

Purity/Quality:

98%min ^*data from raw suppliers

2,3-Naphthalenedicarboximide ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-37/39

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Uses: 2,3-Naphthalenedicarboximide is a useful intermediate. Dyes and metabolites.

Technology Process of 2,3-NAPHTHALENEDICARBOXIMIDE

There total 14 articles about 2,3-NAPHTHALENEDICARBOXIMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2,3-Naphthalenedicarboxylic anhydride (716-39-2) → 2,3-Naphthalimide (4379-54-8)

Guidance literature:

With urea; at 170 ℃; for 2h;

DOI:10.1016/j.bmc.2020.115343

Reference yield: 90.0%

2,3-Naphthalenedicarboxylic anhydride (716-39-2) + urea (57-13-6) → 2,3-Naphthalimide (4379-54-8)

Guidance literature:

at 170 ℃; for 2h;

Reference yield: 88.0%

naphthalene-2,3-dicarboxylic acid (2169-87-1) → 2,3-Naphthalimide (4379-54-8)

Guidance literature:

With urea; In ethylene glycol; at 180 ℃;

upstream raw materials:

2,3-Naphthalenedicarboxylic anhydride

urea

maleiimide

1,2-bis(dibromomethyl)benzene

Downstream raw materials:

2,3-naphthalocyanine

zinc meso-tetraphenyltetra[2,3]naphthaloporphyrine

Refernces

• 1、 -. "SMALL MOLECULE DIRECT INHIBITORS OF KEAP1-NRF2 PROTEIN-PROTEIN INTERACTION". Paragraph 0095-0096. . Retrieved 2020/07/31.
• 2、 Zhang, Yang,Torker, Sebastian,Sigrist, Michel,Bregovi?, Nikola,Dydio, Pawe?. "Binuclear Pd(I)-Pd(I) Catalysis Assisted by Iodide Ligands for Selective Hydroformylation of Alkenes and Alkynes". supporting information. p. 18251 - 18265. Retrieved 2020/11/02.