4-N-BUTYLPHENYLMAGNESIUM BROMIDE

Base Information

• Chemical Name: 4-N-BUTYLPHENYLMAGNESIUM BROMIDE
• CAS No.: 185416-14-2
• Molecular Formula: C10H13 Br Mg
• Molecular Weight: 237.422
• Mol file: 185416-14-2.mol

Synonyms:4-Butylphenylmagnesiumbromide

Chemical Property of 4-N-BUTYLPHENYLMAGNESIUM BROMIDE

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 0.00000
• Density: g/cm³
• LogP: 3.67500

Purity/Quality:

4-n-Butylphenylmagnesiumbromide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-N-BUTYLPHENYLMAGNESIUM BROMIDE

There total 2 articles about 4-N-BUTYLPHENYLMAGNESIUM BROMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-bromobutylbenzene (41492-05-1) + magnesium (7439-95-4) → 4-(1-butyl)phenylmagnesium bromide (185416-14-2)

Guidance literature:

In tetrahydrofuran;

Reference yield:

p-bromobutylbenzene (41492-05-1) → 4-(1-butyl)phenylmagnesium bromide (185416-14-2)

Guidance literature:

With magnesium; In tetrahydrofuran;

DOI:10.1002/adsc.201600535

Reference yield: 99.0%

4-(1-butyl)phenylmagnesium bromide (185416-14-2) + [5,6]fullerene-C70 (741268-81-5,741268-84-8,133227-82-4,133320-10-2,133320-11-3,133869-47-3,134054-62-9,134932-61-9,149820-05-3,149820-06-4,157903-26-9,175779-21-2,115383-22-7,958017-68-0,958017-71-5,958017-74-8,958017-77-1,958017-80-6,140630-87-1,140694-21-9,151716-50-6,157008-89-4,220062-79-3,220062-83-9) → C100H40

Guidance literature:

4-(1-butyl)phenylmagnesium bromide; With copper(I) bromide dimethylsulfide complex; In tetrahydrofuran; at 28 ℃; for 0.333333h;

[5,6]fullerene-C₇₀; In tetrahydrofuran; 1,2-dichloro-benzene; at 45 ℃; for 40h;

With ammonium chloride; In tetrahydrofuran; 1,2-dichloro-benzene;

DOI:10.1021/cm301238n

upstream raw materials:

p-bromobutylbenzene

magnesium

Downstream raw materials:

[2-(4-Butyl-phenyl)-6-methoxy-benzo[b]thiophen-3-yl]-[4-(2-piperidin-1-yl-ethoxy)-phenyl]-methanone

1-[4,6-di-O-(tert-butyldimethylsilyl)-2,3-dideoxy-β-D-erythro-hex-2-enopyranosyl]-4-n-butylbenzene

C₄₃H₅₂O₂S₂

C₅₀H₆₆O₂S₂

Refernces

• 1、 -. "Facile synthesis of a series of liquid crystalline 2-(4'-alkylphenyl)-5-cyanopyridines". Page/Page column 2. . Retrieved 2008/12/06.