2-ethenyl-5-methoxybenzamide

Base Information Edit

Chemical Name:2-ethenyl-5-methoxybenzamide
CAS No.:131002-08-9
Molecular Formula:C₁₀H₁₁NO₂
Molecular Weight:177.203
Hs Code.:
Mol file:131002-08-9.mol

Synonyms:2-ethenyl-5-methoxybenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-ethenyl-5-methoxybenzamide Edit

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Technology Process of 2-ethenyl-5-methoxybenzamide

There total 2 articles about 2-ethenyl-5-methoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 74-85-1
ethene

: 99848-43-8
2-bromo-5-methoxybenzamide

: 131002-08-9
2-ethenyl-5-methoxybenzamide

Guidance literature:: With triethylamine; tris-(o-tolyl)phosphine; palladium diacetate; In acetonitrile; at 120 ℃; for 24h; under 22800 Torr;

Reference yield:

: 7486-35-3
tri-n-butyl(vinyl)tin

: O-Methyl 3-methoxybenzohydroxamate

: C₁₀H₁₁NO₂

: 131002-08-9
2-ethenyl-5-methoxybenzamide

Guidance literature:: With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; cesium acetate; In methanol; at 30 ℃; for 8h; Overall yield = 75 %; Inert atmosphere; Schlenk technique; Sealed tube;
DOI:10.1039/c5cc04211a