Technology Process of methyl 4-undecanoylbenzoate
There total 3 articles about methyl 4-undecanoylbenzoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
methyl 4-(isopropylcarbamoyl)benzoate;
With
2-fluoropyridine; trifluoromethylsulfonic anhydride;
In
dichloromethane;
at -78 - 0 ℃;
Inert atmosphere;
n-decylmagnesium chloride;
In
dichloromethane;
at -20 ℃;
for 0.416667h;
Inert atmosphere;
With
hydrogenchloride; water;
In
tetrahydrofuran; dichloromethane;
at 65 ℃;
for 2h;
chemoselective reaction;
Inert atmosphere;
DOI:10.1038/nchem.1268
- Guidance literature:
-
With
(3-phenylallyl)(chloro)-[1,3-bis(2,6-diisopropylphenyl)-4,5-dihydroimidazol-2-ylidene]palladium(II); potassium carbonate;
In
tetrahydrofuran;
at 23 ℃;
for 15h;
chemoselective reaction;
Schlenk technique;
Inert atmosphere;
DOI:10.1021/acs.orglett.8b02911
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrahydrofuran / 15 h / 20 °C
2: (3-phenylallyl)(chloro)-[1,3-bis(2,6-diisopropylphenyl)-4,5-dihydroimidazol-2-ylidene]palladium(II); potassium carbonate / tetrahydrofuran / 15 h / 23 °C / Schlenk technique; Inert atmosphere
With
(3-phenylallyl)(chloro)-[1,3-bis(2,6-diisopropylphenyl)-4,5-dihydroimidazol-2-ylidene]palladium(II); potassium carbonate;
In
tetrahydrofuran;
2: |Suzuki-Miyaura Coupling;
DOI:10.1021/acs.orglett.8b02911
