Benzaldehyde, 4-(ethylamino)- (9CI)

Base Information

• Chemical Name: Benzaldehyde, 4-(ethylamino)- (9CI)
• CAS No.: 79865-89-7
• Molecular Formula: C9H11 N O
• Molecular Weight: 149.192
• Hs Code.: 2922399090
• Mol file: 79865-89-7.mol

Synonyms:p-(Ethylamino)benzaldehyde

Chemical Property of Benzaldehyde, 4-(ethylamino)- (9CI)

Chemical Property:

• PSA: 29.10000
• LogP: 2.00390
• Storage Temp.: under inert gas (nitrogen or Argon) at 2–8 °C

Purity/Quality:

99%, ^*data from raw suppliers

4-Ethylamino-benzaldehyde 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzaldehyde, 4-(ethylamino)- (9CI)

There total 16 articles about Benzaldehyde, 4-(ethylamino)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

N-Ethyl-2-(4-formyl-phenoxy)-acetamide → 4-(ethylamino)benzaldehyde (79865-89-7)

Guidance literature:

With potassium hydroxide; In toluene; for 4h; Heating;

Reference yield: 42.0%

4-fluorobenzaldehyde (459-57-4) + ethylamine (75-04-7,85404-22-4) → 4-(ethylamino)benzaldehyde (79865-89-7)

Guidance literature:

With tetrabutylammomium bromide; potassium carbonate; In dimethyl sulfoxide; at 90 ℃; for 48h;

DOI:10.1002/ejoc.201700805

Reference yield: 21.0%

ethanamine hydrochloride (557-66-4) + 4-methoxy-benzaldehyde (123-11-5) → 4-(ethylamino)benzaldehyde (79865-89-7)

Guidance literature:

With triethylamine;

upstream raw materials:

N-ethyl-N-phenylamine

p,p'-diaminobiphenyl

ethanamine hydrochloride

4-methoxy-benzaldehyde

Downstream raw materials:

1-<4-Aethylamino-benzyliden>-inden

2-(4-(ethylamino)benzylidene)-6-hydroxy-5-methoxy-2,3-dihydro-1H-inden-1-one hydrochloride

2-(4-(ethyl(methyl)amino)benzylidene)-6-hydroxy-5-methoxy-2,3-dihydro-1H-inden-1-one hydrochloride

2-(4-(ethyl(methyl)amino)benzylidene)-5,6-dihydroxy-2,3-dihydro-1H-inden-1-one 4-methylbenzene-1-sulfonic acid

Refernces

• 1、 Wang, Jing,Qi, Tianqinji,Li, Zhibin,She, Wei,Li, Xuewei,Li, Jingfang,Yan, Pengfei,Li, Weizuo,Li, Guangming. "A strategy of two-step tandem catalysis towards direct N-alkylation of nitroarenes with ethanol via facile fabricated novel Co-based catalysts derived from coordination polymers". . p. 106 - 118. Retrieved 2019/07/19.
• 2、 Wang, Bingshuai,Yu, Fabiao,Li, Peng,Sun, Xiaofei,Han, Keli. "A BODIPY fluorescence probe modulated by selenoxide spirocyclization reaction for peroxynitrite detection and imaging in living cells". . p. 383 - 390. Retrieved 2013/02/22.