3-Bromopropionamide

Base Information

• Chemical Name: 3-Bromopropionamide
• CAS No.: 6320-96-3
• Molecular Formula: C3 H6 Br N O
• Molecular Weight: 151.991
• Hs Code.: 2924199090
• Mol file: 6320-96-3.mol

Synonyms:Propionamide,3-bromo- (6CI);3-Bromopropionamide 98+%;Bromopropionamide;

Chemical Property of 3-Bromopropionamide

Chemical Property:

• Melting Point: 113 ºC
• Boiling Point: 303.1 ºC at 760 mmHg
• PKA: 15.95±0.40(Predicted)
• Flash Point: 137.1 ºC
• PSA: 43.09000
• Density: 1.651 g/cm³
• LogP: 0.95700
• Storage Temp.: 2-8°C
• Water Solubility.: almost transparency

Purity/Quality:

99% ^*data from raw suppliers

3-Bromopropionamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xn
• Hazard Codes: Xn
• Statements: 22-51
• Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Bromopropionamide

There total 7 articles about 3-Bromopropionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

→ methyl bromide (74-83-9) + 3-bromopropanamide (6320-96-3)

Guidance literature:

Reference yield:

3-Bromopropionyl chloride (15486-96-1) → 3-bromopropanamide (6320-96-3)

Guidance literature:

With ammonia; at -10 ℃;

Reference yield:

3-chloropropionamide (5875-24-1) → 3-bromopropanamide (6320-96-3)

Guidance literature:

With lithium bromide; In various solvent(s); at 120 ℃; for 2h; Yield given;

DOI:10.1080/00397919408012653

upstream raw materials:

3-bromopropanoyl isocyanate

3-Bromopropionyl chloride

3-Bromo-propionimidic acid ethyl ester

3-chloropropionamide

Downstream raw materials:

α-(1-phenylpyrazolo<3,4-d>pyrimidin-4-ylthio)propionamide

3-[7-(4-Methoxy-benzyl)-2,6-dioxo-3-propyl-2,3,6,7-tetrahydro-purin-1-yl]-propionamide

Propionamid

Refernces

• 1、 Martin,Bartlett. "-". . p. 2533,2540. Retrieved 1957.
• 2、 Lind, Johan,Jonsson, Mats,Xinhua, Shen,Eriksen, Trygve E.,Merényi, Gábor,Eberson, Lennart. "Kinetics of radical-initiated chain bromination of 2-methyl-2-propanol by N-bromosuccinimide in water". . p. 3503 - 3510. Retrieved 2007/10/02.