phenyl dehydroselenoabietate

Base Information

• Chemical Name: phenyl dehydroselenoabietate
• CAS No.: 76932-72-4
• Molecular Formula: C₂₆H₃₂OSe
• Molecular Weight: 439.499
• Mol file: 76932-72-4.mol

Synonyms:

Chemical Property of phenyl dehydroselenoabietate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of phenyl dehydroselenoabietate

There total 2 articles about phenyl dehydroselenoabietate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dehydroabietic acid (1740-19-8) → phenyl dehydroselenoabietate (76932-72-4)

Guidance literature:

Multi-step reaction with 2 steps

1: oxalyl chloride / benzene / 1 h / 0 °C

2: pyridine / tetrahydrofuran; benzene / 0.75 h / Ambient temperature

With pyridine; oxalyl dichloride; In tetrahydrofuran; benzene;

DOI:10.1002/hlca.19800630823

Reference yield:

dehydroabietic acid chloride (22478-66-6) + Benzeneselenol (645-96-5) → phenyl dehydroselenoabietate (76932-72-4)

Guidance literature:

With pyridine; In tetrahydrofuran; benzene; for 0.75h; Yield given; Ambient temperature;

DOI:10.1002/hlca.19800630823

Reference yield: 96.0%

phenyl dehydroselenoabietate (76932-72-4) → 18-Norabieta-8,11,13-triene (5323-56-8,19407-17-1,19407-18-2,32298-75-2,32367-41-2)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; at 80 ℃;

DOI:10.1002/hlca.19800630823

upstream raw materials:

dehydroabietic acid chloride

Benzeneselenol

dehydroabietic acid

Downstream raw materials:

18-Norabieta-8,11,13-triene

Refernces