Technology Process of C50H96O2
There total 7 articles about C50H96O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Br(1-)*C37H52O2P(1+);
With
sodium hexamethyldisilazane;
In
tetrahydrofuran;
at 20 ℃;
C31H60O;
In
tetrahydrofuran;
at -84 ℃;
diastereoselective reaction;
DOI:10.1016/j.tetlet.2011.11.021
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: acetonitrile / 170 °C / Microwave irradiation
2.1: sodium hexamethyldisilazane / tetrahydrofuran / 20 °C
2.2: -84 °C
With
sodium hexamethyldisilazane;
In
tetrahydrofuran; acetonitrile;
2.1: Wittig reaction / 2.2: Wittig reaction;
DOI:10.1016/j.tetlet.2011.11.021
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: methanol; toluene-4-sulfonic acid / dichloromethane
2.1: sulfuric acid; water; hydrogen bromide / 110 °C
3.1: acetonitrile / 170 °C / Microwave irradiation
4.1: sodium hexamethyldisilazane / tetrahydrofuran / 20 °C
4.2: -84 °C
With
methanol; sulfuric acid; water; hydrogen bromide; sodium hexamethyldisilazane; toluene-4-sulfonic acid;
In
tetrahydrofuran; dichloromethane; acetonitrile;
4.1: Wittig reaction / 4.2: Wittig reaction;
DOI:10.1016/j.tetlet.2011.11.021