benzyl 2-butenyl sulfone

Base Information

• Chemical Name: benzyl 2-butenyl sulfone
• CAS No.: 134988-46-8
• Molecular Formula: C₁₁H₁₄O₂S
• Molecular Weight: 210.297
• Mol file: 134988-46-8.mol

Synonyms:

Chemical Property of benzyl 2-butenyl sulfone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of benzyl 2-butenyl sulfone

There total 4 articles about benzyl 2-butenyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

benzyl 4-chlorobutyl sulfone (14633-43-3) → 2-phenyltetrahydro-2H-thiopyran 1,1-dioxide (14856-64-5) + benzyl 2-butenyl sulfone (134988-46-8) + benzyl 3-butenyl sulfone (50675-40-6) + benzyl cyclobutyl sulfone (134988-47-9)

Guidance literature:

With sodium hydroxide; tetrabutylammomium bromide; In benzene; at 100 ℃; for 12h;

Reference yield:

benzyl but-2-enyl sulfide (31409-96-8) → benzyl 2-butenyl sulfone (134988-46-8)

Guidance literature:

With dihydrogen peroxide; acetic acid;

Reference yield:

benzyl chloride (100-44-7) → benzyl 2-butenyl sulfone (134988-46-8)

Guidance literature:

Multi-step reaction with 2 steps

2: aqueous H₂O₂; acetic acid

With dihydrogen peroxide; acetic acid;

upstream raw materials:

benzyl but-2-enyl sulfide

benzyl 4-chlorobutyl sulfone

benzyl chloride

phenylmethanethiol

Downstream raw materials:

(butylsulfonyl)methylbenzene

Refernces