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1000623-98-2

Basic Information
CAS No.: 1000623-98-2
Name: 2,5-Di(HD)-3,6-di(5-broMothiophen)diketopyrrolopyrrole
Article Data: 7
Molecular Structure:
Molecular Structure of 1000623-98-2 (2,5-Di(HD)-3,6-di(5-broMothiophen)diketopyrrolopyrrole)
Formula: C46H70Br2N2O2S2
Molecular Weight: 907.014
Synonyms: 2,5-Di(HD)-3,6-di(5-broMothiophen)diketopyrrolopyrrole;3,6-Bis(5-broMo-2-thienyl)-2,5-bis(2-hexyldecyl)pyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione;3,6-bis(5-broMo-2-thienyl)-2,5-bis(2-hexyldecyl)-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione DPP-iC16;Pyrrolo[3,4-c]pyrrole-1,4-dione,3,6-bis(5-bromo-2-thienyl)-2-5-bis(2-hexyldecyl)-2,5-dihydro-;3,6-bis(5-bromothiophen-2-yl)-2,5-bis(2-hexyldecyl)pyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione;3,6-Bis(5-bromo-2-thienyl)-2,5-bis(2-hexyldecyl)-2,5-dihydro-pyrrolo[3,4-c]pyrrole-1,4-dione 98%
EINECS: -0
Density: 1.24±0.1 g/cm3(Predicted)
Melting Point: 110-115°C
Boiling Point: 865.4±65.0 °C(Predicted)
PSA: 100.48000
LogP: 16.20900
Synthetic route
1044598-80-2

3,6-bis(5-bromothien-2-yl)-2,5-bis(2-hexyldecyl)pyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione

1000623-98-2

3,6-bis(5-bromo-2-thienyl)-2,5-dihydro-2,5-di(2'-hexyldecyl)-pyrrolo[3,4c]pyrrolo-1,4-dione

Conditions
ConditionsYield
With N-Bromosuccinimide In chloroform at 50℃; for 2h; Inert atmosphere;79.9%
With N-Bromosuccinimide In chloroform for 48h; Darkness;61%
With N-Bromosuccinimide In chloroform for 48h; Darkness;60%
1044598-80-2

3,6-bis(5-bromothien-2-yl)-2,5-bis(2-hexyldecyl)pyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione

A

1000623-98-2

3,6-bis(5-bromo-2-thienyl)-2,5-dihydro-2,5-di(2'-hexyldecyl)-pyrrolo[3,4c]pyrrolo-1,4-dione

B

1423138-95-7

3-(5-bromothiophen-2-yl)-2,5-bis(2-hexyldecyl)-6-(thiophen-2-yl)pyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione

Conditions
ConditionsYield
With N-Bromosuccinimide In chloroform at 0 - 20℃; Darkness;A 17%
B 56%

3,6-dithiophen-2-yl-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione

1044598-79-9

7-(iodomethyl)pentadecane

1000623-98-2

3,6-bis(5-bromo-2-thienyl)-2,5-dihydro-2,5-di(2'-hexyldecyl)-pyrrolo[3,4c]pyrrolo-1,4-dione

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: potassium carbonate / N,N-dimethyl-formamide / 120 °C
2: N-Bromosuccinimide / chloroform / 20 °C
View Scheme
1003-31-2

thiophene-2-carbonitrile

1000623-98-2

3,6-bis(5-bromo-2-thienyl)-2,5-dihydro-2,5-di(2'-hexyldecyl)-pyrrolo[3,4c]pyrrolo-1,4-dione

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: sodium / tert-Amyl alcohol / 120 °C
2: potassium carbonate / N,N-dimethyl-formamide / 120 °C
3: N-Bromosuccinimide / chloroform / 20 °C
View Scheme
Multi-step reaction with 3 steps
1: potassium tert-butylate / tert-Amyl alcohol / 4 h / 110 °C
2: potassium carbonate / N,N-dimethyl-formamide / 24 h / 110 °C
3: N-Bromosuccinimide / chloroform / 48 h / Darkness
View Scheme
Multi-step reaction with 3 steps
1.1: potassium tert-butylate / tert-Amyl alcohol / 5 h / 110 °C / Inert atmosphere
2.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 130 °C / Inert atmosphere
2.2: 130 °C / Inert atmosphere
3.1: N-Bromosuccinimide / chloroform / 2 h / 50 °C / Inert atmosphere
View Scheme
2425-77-6

2-hexyldecan-1-ol

1000623-98-2

3,6-bis(5-bromo-2-thienyl)-2,5-dihydro-2,5-di(2'-hexyldecyl)-pyrrolo[3,4c]pyrrolo-1,4-dione

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1H-imidazole; iodine; triphenylphosphine / dichloromethane / 20 °C
2: potassium carbonate / N,N-dimethyl-formamide / 120 °C
3: N-Bromosuccinimide / chloroform / 20 °C
View Scheme

3,6-dithiophen-2-yl-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione

1000623-98-2

3,6-bis(5-bromo-2-thienyl)-2,5-dihydro-2,5-di(2'-hexyldecyl)-pyrrolo[3,4c]pyrrolo-1,4-dione

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 110 °C
2: N-Bromosuccinimide / chloroform / 48 h / Darkness
View Scheme
1000623-98-2

3,6-bis(5-bromo-2-thienyl)-2,5-dihydro-2,5-di(2'-hexyldecyl)-pyrrolo[3,4c]pyrrolo-1,4-dione

24388-23-6

2-phenyl-4,4,5,5-tetramethyl-1,3,2-dioxoborole

2,5-bis(2-hexyldecyl)-3,6-bis(5-phenylthiophen-2-yl)-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione

Conditions
ConditionsYield
Stage #1: 3,6-bis(5-bromo-2-thienyl)-2,5-dihydro-2,5-di(2'-hexyldecyl)-pyrrolo[3,4c]pyrrolo-1,4-dione; 2-phenyl-4,4,5,5-tetramethyl-1,3,2-dioxoborole With tris-(dibenzylideneacetone)dipalladium(0); Aliquat (at)366; triphenylphosphine In water; toluene for 0.25h; Schlenk technique; Inert atmosphere;
Stage #2: With potassium phosphate In water; toluene at 115℃; for 16h; Schlenk technique; Inert atmosphere; Sealed tube;
97%
1000623-98-2

3,6-bis(5-bromo-2-thienyl)-2,5-dihydro-2,5-di(2'-hexyldecyl)-pyrrolo[3,4c]pyrrolo-1,4-dione

24388-23-6

2-phenyl-4,4,5,5-tetramethyl-1,3,2-dioxoborole

A

2,5-bis(2-hexyldecyl)-3,6-bis(5-phenylthiophen-2-yl)-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione

B

C104H150N4O4S4

Conditions
ConditionsYield
Stage #1: 3,6-bis(5-bromo-2-thienyl)-2,5-dihydro-2,5-di(2'-hexyldecyl)-pyrrolo[3,4c]pyrrolo-1,4-dione; 2-phenyl-4,4,5,5-tetramethyl-1,3,2-dioxoborole With tris-(dibenzylideneacetone)dipalladium(0); Aliquat (at)366; triphenylphosphine In water; toluene Schlenk technique; Inert atmosphere;
Stage #2: With potassium phosphate In water; toluene at 115℃; Schlenk technique; Inert atmosphere; Sealed tube;
A 87%
B 6.6%
1000623-98-2

3,6-bis(5-bromo-2-thienyl)-2,5-dihydro-2,5-di(2'-hexyldecyl)-pyrrolo[3,4c]pyrrolo-1,4-dione

78053-56-2

2-Ethynylanthracene

3,6-bis(5-(anthracen-2-ylethynyl)thiophen-2-yl)-2,5-bis(2-hexyldecyl)pyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione

Conditions
ConditionsYield
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); N-ethyl-N,N-diisopropylamine In toluene at 60℃; for 8h; Sonogashira Cross-Coupling; Inert atmosphere; Schlenk technique;75%
1000623-98-2

3,6-bis(5-bromo-2-thienyl)-2,5-dihydro-2,5-di(2'-hexyldecyl)-pyrrolo[3,4c]pyrrolo-1,4-dione

1625689-09-9

C15H15BF2N2

C76H98B2F4N6O2S2

Conditions
ConditionsYield
Stage #1: 3,6-bis(5-bromo-2-thienyl)-2,5-dihydro-2,5-di(2'-hexyldecyl)-pyrrolo[3,4c]pyrrolo-1,4-dione With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); N-ethyl-N,N-diisopropylamine In tetrahydrofuran Schlenk technique; Inert atmosphere;
Stage #2: C15H15BF2N2 In tetrahydrofuran at 60℃; for 3h; Inert atmosphere;
75%
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    Product Name: 2,5-Di(HD)-3,6-di(5-broMothiophen)diketopyrrolopyrrole Synonyms: 2,5-Di(HD)-3,6-di(5-broMothiophen)diketopyrrolopyrrole;3,6-Bis(5-broMo-2-thienyl)-2,5-bis(2-hexyldecyl)pyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione;3,6-bis(5-broMo-2-thien

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    factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

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  •  Changzhou Helios Biomedical Science and Technology Co.,LTD.

     China (Mainland)  |  Contact Details

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  • 2,5-Di(HD)-3,6-di(5-broMothiophen)diketopyrrolopyrrole

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    1000623-98-2

    2,5-Di(HD)-3,6-di(5-broMothiophen)diketopyrrolopyrrole

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    factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

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    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86 19334956669

    Address:Waisha Road,Jiaojiang

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  • 3,6-Bis(5-bromo-2-thienyl)-2,5-bis(2-hexyldecyl)pyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione

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    1000623-98-2

    3,6-Bis(5-bromo-2-thienyl)-2,5-bis(2-hexyldecyl)pyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione

    Min.Order: 10 Milligram

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    1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

    Founded in 2011, Amadis Chemical Company Limited is an innovative manufacturer of chemical products and technical service providers. Our business includes sales, manufacture, and s

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    Business Type:Lab/Research institutions

    Tel:86-571-89925085

    Address:Watts Cosine.No.166.Xiangmao Road.

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  • Factory price photoelectric material 1000623-98-2

  • Casno:

    1000623-98-2

    Factory price photoelectric material 1000623-98-2

    Min.Order: 1 Metric Ton

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    Appearance:powder Storage:Refrigerator Package:Depended Application:150600-72-9 Transportation:by air or by sea Port:China Main Port

    Henan Sunlake Enterprise Corporation is located in Henan Province , the central plain of China , which enjoys favorable geogeaphical position and convenient transportion. The compa

  • HENAN SUNLAKE ENTERPRISE CORPORATION

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-371- 86259723

    Address:Mingmen International Center, NO.222 Dongming Road,Zhengzhou,Henan,China

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  • National Research Platform  ISO 9001  1000623-98-2

  • Casno:

    1000623-98-2

    National Research Platform ISO 9001 1000623-98-2

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    1. Subsidiary of Institute of Chemistry, Henan Academy of Sciences, national research platform;2. About 30 years’ experience in this field since 1983;3. An experienced R&D team consisting of Doctors and Masters;4. Various types of analytical instrume

    Zhengzhou Kingorgchem Chemical Technology Co., Ltd. was founded on the basis of Organophosphorus Chemistry Lab of Institute of Chemistry Henan Academy of Sciences in 2015. The

  • Zhengzhou Kingorgchem Chemical Technology Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-371-65511936

    Address:NO.56,Hongzhuan Road

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  • 1000623-98-2

  • Casno:

    1000623-98-2

    1000623-98-2

    Min.Order: 0

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    Nanjing Chemlin Chemical Industry Co., Ltd was established in Aug,1999, located in the industrial park of Nanjing University of Technology, It is a private enterprises in Jiangsu Province with 1200 square meters’ R&D center. Our R&D center has a well

    Nanjing Chemlin Chemical Industry Co., Ltd was established in Aug,1999, located in the industrial park of Nanjing University of Technology, It is a private enterprises in Jiangsu P

  • Nanjing Chemlin Chemical Co., Ltd.

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-25-83697070

    Address:Rm.902 Longyin Plaza, No. 217 Zhongshan Rd.(N) Nanjing 210009,China

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  • 3,6-Bis(5-bromothiophen-2-yl)-2,5-bis(2-hexyldecyl)pyrrolo[3,4-c] pyrrole-1,4(2H,5H)-dione

  • Casno:

    1000623-98-2

    3,6-Bis(5-bromothiophen-2-yl)-2,5-bis(2-hexyldecyl)pyrrolo[3,4-c] pyrrole-1,4(2H,5H)-dione

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    This chemical is produced by SunaTech Inc., which is high purity, stable quality, long-term supply, etc. We also provide service of custom synthesis according to your request. Package:Glass vials/bottles wrapped with aluminum foil bag package. For li

    SunaTech Inc., located in Suzhou Industrial Park, Jiangsu, China, is committed to providing support to the research and development of advanced technologies that ultimately benef

  • SunaTech Inc.

     China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:+86 512 6287 2180

    Address:398 Ruoshui Road, Suzhou Industrial Park, Suzhou, Jiangsu, P. R. China

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  • 3,6-dibromo-7-hydroxy-8-quinolinecarboxylic acid

  • Casno:

    1000623-98-2

    3,6-dibromo-7-hydroxy-8-quinolinecarboxylic acid

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Debyesci is here who supplied several kinds of chemical products to global pharmaceutical, drug discovery, agrochemical and biotechnology industries for four yearsOur key scientific leadership team has gained experience in top research and developmen

    Debyesci is here who supplied several kinds of chemical products to global pharmaceutical, drug discovery, agrochemical and biotechnology industries for four years Our key scienti

  • Debye Scientific

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+85221376140

    Address:Rm. 19C, Lockhart Ctr., 301-307 Lockhart Rd., Wan Chai

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