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CAS No.: | 111050-72-7 |
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Name: | 1-((3,5-dichloro)-2,6-dihydroxy-4-methoxyphenyl)-1-hexanone |
Article Data: | 4 |
Molecular Structure: | |
Formula: | C13H16Cl2O4 |
Molecular Weight: | 307.174 |
Synonyms: | 1-((3,5-dichloro)-2,6-dihydroxy-4-methoxyphenyl)-1-hexanone |
Density: | 1.325g/cm3 |
Boiling Point: | 434.3°Cat760mmHg |
Flash Point: | 216.5°C |
PSA: | 66.76000 |
LogP: | 4.17620 |
1-(2,6-dihydroxy-4-methoxyphenyl)hexan-1-one
1-(3,5-dichloro-2,6-dihydroxy-4-methoxyphenyl)hexane-1-one
Conditions | Yield |
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With sulfuryl dichloride In methanol; dichloromethane at 20℃; | 100% |
With sulfuryl dichloride In ethanol; chloroform at 20℃; for 1h; | 93% |
With sulfuryl dichloride In ethanol; chloroform at 20℃; for 1h; | 93% |
With sulfuryl dichloride In methanol; dichloromethane at 20℃; for 0.333333h; |
5-methoxyresorcinol
1-(3,5-dichloro-2,6-dihydroxy-4-methoxyphenyl)hexane-1-one
Conditions | Yield |
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Multi-step reaction with 2 steps 1: 58 percent / AlCl3 / CH2Cl2 / 3 h / 20 °C 2: 93 percent / SO2Cl2 / ethanol; CHCl3 / 1 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: aluminum (III) chloride / dichloromethane / 20 °C 2: sulfuryl dichloride / ethanol; chloroform / 1 h / 20 °C View Scheme |
Hexanoyl chloride
1-(3,5-dichloro-2,6-dihydroxy-4-methoxyphenyl)hexane-1-one
Conditions | Yield |
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Multi-step reaction with 2 steps 1: 58 percent / AlCl3 / CH2Cl2 / 3 h / 20 °C 2: 93 percent / SO2Cl2 / ethanol; CHCl3 / 1 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: aluminum (III) chloride / dichloromethane / 20 °C 2: sulfuryl dichloride / ethanol; chloroform / 1 h / 20 °C View Scheme |
1-(3,5-dichloro-2,6-dihydroxy-4-methoxyphenyl)hexane-1-one
Conditions | Yield |
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With triethylsilane; trifluoroacetic acid at 20℃; for 8h; | 96% |
methyl p-toluene sulfonate
1-(3,5-dichloro-2,6-dihydroxy-4-methoxyphenyl)hexane-1-one
Conditions | Yield |
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With potassium carbonate In acetone at 20℃; for 16h; | 95% |
With potassium carbonate at 20℃; for 16h; | 95% |
1-(3,5-dichloro-2,6-dihydroxy-4-methoxyphenyl)hexane-1-one
(3,5-dichloro-2,4,6-trihydroxyphenyl)-1-hexan-1-one
Conditions | Yield |
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With boron tribromide In dichloromethane for 16h; | 40% |