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1315478-13-7

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Basic Information
CAS No.: 1315478-13-7
Name: 2-(2-butyl-4-hydroxy-6-MethylpyriMidin-5-yl)-N,N-diMethylacetaMide
Article Data: 5
Molecular Structure:
Molecular Structure of 1315478-13-7 (2-(2-butyl-4-hydroxy-6-MethylpyriMidin-5-yl)-N,N-diMethylacetaMide)
Formula: C13H21N3O2
Molecular Weight: 251.329
Synonyms: 2-Butyl-1,6-dihydro-N,N,4-trimethyl-6-oxo-5-pyrimidineacetamide;
Density: 1.11±0.1 g/cm3(Predicted)
Boiling Point: 385.0±44.0 °C(Predicted)
PSA: 66.32000
LogP: 1.46390
Related products
Synthetic route
1315478-16-0

2-(2-n-butyl-4-hydroxy-6-methyl-pyrimidin-5-yl)acetic acid

506-59-2

N,N-dimethylammonium chloride

1315478-13-7

(2-(2-n-butyl-4-hydroxy-6-methyl-pyrimidin-5-yl)-N,N-dimethylacetamide)

Conditions
ConditionsYield
Stage #1: 2-(2-n-butyl-4-hydroxy-6-methyl-pyrimidin-5-yl)acetic acid With triethylamine In dichloromethane at 0℃; for 0.5h;
Stage #2: N,N-dimethylammonium chloride With chloroformic acid ethyl ester In dichloromethane for 12h; Reflux;
Stage #3: With sodium hydroxide In dichloromethane; water pH=9;		93%
With 4-methyl-morpholine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 5h; Inert atmosphere;86%
1315478-16-0

2-(2-n-butyl-4-hydroxy-6-methyl-pyrimidin-5-yl)acetic acid

124-40-3

dimethyl amine

1315478-13-7

(2-(2-n-butyl-4-hydroxy-6-methyl-pyrimidin-5-yl)-N,N-dimethylacetamide)

Conditions
ConditionsYield
Stage #1: 2-(2-n-butyl-4-hydroxy-6-methyl-pyrimidin-5-yl)acetic acid With 4-methyl-morpholine In N,N-dimethyl acetamide for 0.166667h;
Stage #2: With 1,1'-carbonyldiimidazole In N,N-dimethyl acetamide at 20℃; for 1h;
Stage #3: dimethyl amine In tetrahydrofuran; N,N-dimethyl acetamide at 20℃; for 0.5h; Solvent; Concentration;		87.2%
1315478-14-8

methyl 2-(N,N-dimethylaminocarbonylmethyl)acetoacetate

18257-46-0

pentanamidine hydrochloride

1315478-13-7

(2-(2-n-butyl-4-hydroxy-6-methyl-pyrimidin-5-yl)-N,N-dimethylacetamide)

Conditions
ConditionsYield
Stage #1: pentanamidine hydrochloride With sodium hydroxide In methanol for 0.5h; Cooling with ice;
Stage #2: methyl 2-(N,N-dimethylaminocarbonylmethyl)acetoacetate In methanol at 30℃; for 10h; Cooling with ice;		71.7%
With ethanol; potassium hydroxide at 25℃; for 15h;70%
1315478-15-9

ethyl 2-(N,N-dimethylaminocarbonylmethyl)acetoacetate

18257-46-0

pentanamidine hydrochloride

1315478-13-7

(2-(2-n-butyl-4-hydroxy-6-methyl-pyrimidin-5-yl)-N,N-dimethylacetamide)

Conditions
ConditionsYield
Stage #1: pentanamidine hydrochloride With sodium hydroxide In ethanol for 0.5h; Cooling with ice;
Stage #2: ethyl 2-(N,N-dimethylaminocarbonylmethyl)acetoacetate In methanol at 30℃; for 10h; Cooling with ice;		50.3%
With ethanol; potassium hydroxide at 25℃; for 4h;47%
110-59-8

pentanonitrile

1315478-13-7

(2-(2-n-butyl-4-hydroxy-6-methyl-pyrimidin-5-yl)-N,N-dimethylacetamide)

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: hydrogenchloride / methanol / 9 h / 0 - 10 °C
1.2: 0 - 20 °C / pH 8.5
2.1: potassium hydroxide / methanol / 15 h / 20 °C
3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4-methyl-morpholine / dichloromethane / 5 h / 0 - 20 °C / Inert atmosphere
View Scheme
1315478-13-7

(2-(2-n-butyl-4-hydroxy-6-methyl-pyrimidin-5-yl)-N,N-dimethylacetamide)

2-(2-n-butyl-4-hydroxy-6-methylpyrimidin-5-yl)-N,N-dimethylthioacetamide

Conditions
ConditionsYield
With Lawessons reagent In toluene at 110℃; for 2h; Inert atmosphere;92%
1315478-13-7

(2-(2-n-butyl-4-hydroxy-6-methyl-pyrimidin-5-yl)-N,N-dimethylacetamide)

114772-54-2

4'-(bromomethyl)-1,1'-biphenyl-2-carbonitrile

C27H30N4O2

Conditions
ConditionsYield
Stage #1: (2-(2-n-butyl-4-hydroxy-6-methyl-pyrimidin-5-yl)-N,N-dimethylacetamide) With lithium hydride In N,N-dimethyl-formamide; toluene at 20℃; for 1h; Inert atmosphere;
Stage #2: 4'-(bromomethyl)-1,1'-biphenyl-2-carbonitrile In N,N-dimethyl-formamide; toluene at 80 - 85℃; for 24h; Reagent/catalyst;		83%
1315478-13-7

(2-(2-n-butyl-4-hydroxy-6-methyl-pyrimidin-5-yl)-N,N-dimethylacetamide)

BR-A-557

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: lithium hydride / toluene; N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere
1.2: 24 h / 80 - 85 °C
2.1: zinc(II) chloride; sodium azide / N,N-dimethyl-formamide / 28 h / 80 - 130 °C / Inert atmosphere
2.2: 0 - 5 °C
View Scheme
1315478-13-7

(2-(2-n-butyl-4-hydroxy-6-methyl-pyrimidin-5-yl)-N,N-dimethylacetamide)

247257-48-3

Fimasartan

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: lithium hydride / toluene; N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere
1.2: 24 h / 80 - 85 °C
2.1: zinc(II) chloride; sodium azide / N,N-dimethyl-formamide / 28 h / 80 - 130 °C / Inert atmosphere
2.2: 0 - 5 °C
3.1: Lawessons reagent / toluene / 3 h / Reflux
View Scheme
Multi-step reaction with 3 steps
1.1: Lawessons reagent / toluene / 2 h / 110 °C / Inert atmosphere
2.1: lithium hydride / N,N-dimethyl-formamide; hexane / 1 h / 0 °C / Inert atmosphere
2.2: 24 h / 70 °C / Inert atmosphere
3.1: acetic acid / tetrahydrofuran; water / 2 h / Reflux
View Scheme
1315478-13-7

(2-(2-n-butyl-4-hydroxy-6-methyl-pyrimidin-5-yl)-N,N-dimethylacetamide)

1361024-52-3

2-n-butyl-5-(N,N-dimethylaminothioformylmethyl)-6-methyl-3-[[2'-(N-triphenylmethyl-5-tetrazolyl)biphenyl]-4-methyl]pyrimidin-4-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: Lawessons reagent / toluene / 2 h / 110 °C / Inert atmosphere
2.1: lithium hydride / N,N-dimethyl-formamide; hexane / 1 h / 0 °C / Inert atmosphere
2.2: 24 h / 70 °C / Inert atmosphere
View Scheme
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  • Casno:

    1315478-13-7

    2-(2-butyl-4-hydroxy-6-MethylpyriMidin-5-yl)-N,N-diMethylacetaMide

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    GIHI CHEMICALS CO.,LIMITED, its former company is a small manufacturer who is specialized in the production of ester products which are used in the daily chemicals ,cosmetic produc

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     China (Mainland)  |  Contact Details

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  • Casno:

    1315478-13-7

    2-(2-Butyl-4-Hydroxy-6-Methylpyrimidin-5-Yl)-N,N-Dimethylacetamide

    Min.Order: 100 Gram

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    Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands

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     China (Mainland)  |  Contact Details

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  • 2-(2-Butyl-4-Hydroxy-6-Methylpyrimidin-5-Yl)-N,N-Dimethylacetamide

  • Casno:

    1315478-13-7

    2-(2-Butyl-4-Hydroxy-6-Methylpyrimidin-5-Yl)-N,N-Dimethylacetamide

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    TAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp

    As a member of TAIHO Group,Hubei Taiho Chemical Co.,Ltd,is a professional new-type chemicals enterprise combined into research and development,production and sales.We adhere to the

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     China (Mainland)  |  Contact Details

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  • 2-(2-butyl-4-hydroxy-6-MethylpyriMidin-5-yl)-N,N-diMethylacetaMide

  • Casno:

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    2-(2-butyl-4-hydroxy-6-MethylpyriMidin-5-yl)-N,N-diMethylacetaMide

    Min.Order: 0

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    J&H CHEM is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other Value-added customer services, for diversified range products of chemicals

    J&H Chemical is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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  • 2-(2-butyl-4-hydroxy-6-MethylpyriMidin-5-yl)-N,N-diMethylacetaMide

  • Casno:

    1315478-13-7

    2-(2-butyl-4-hydroxy-6-MethylpyriMidin-5-yl)-N,N-diMethylacetaMide

    Min.Order: 0

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    1. Product advantages? High purity, all above 98.5%, no impurities after dissolution? We will test each batch to ensure quality? OEM and private brand services designed for free? Various cap colors available? We can also provide MT1 peptide powder2.

    Hebei Sankai Chemical Technology Co., Ltd. is a new chemical enterprise integrating the research, manufacturing and supply of chemicals. Located in the beautiful "cattle city" Xing

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     China (Mainland)  |  Contact Details

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  • 2-(2-butyl-4-methyl-6-oxo-1,6-dihydropyrimidin-5-yl)-N,N-dimethylacetamide

  • Casno:

    1315478-13-7

    2-(2-butyl-4-methyl-6-oxo-1,6-dihydropyrimidin-5-yl)-N,N-dimethylacetamide

    Min.Order: 0

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    Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

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    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    Address:Room1027,No.Jinyu Road,Pudong

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  • 2-(2-butyl-4-hydroxy-6-MethylpyriMidin-5-yl)-N,N-diMethylacetaMide

  • Casno:

    1315478-13-7

    2-(2-butyl-4-hydroxy-6-MethylpyriMidin-5-yl)-N,N-diMethylacetaMide

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    good quality, competitive price, thoughtful after sale serviceAppearance:White to Off-White Solid Storage:Keep it in dry,shady and cool place Package:as your requirement Application:Pharma;Industry;Agricultural;chemical reaserch Transportation:by Sea

    Wuhan Circle Star Bio-medic Technology co.,Ltd is located in wuhan, the central city of China, the core of the Changjiang river economic belt and known as the "thoroughfare of nin

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-13437180835

    Address:Experimental Building 311-15, Nuclear Magnetic Spectrometer Industry Base, No. 128 Guanggu 7th Road, Donghu New Technology Development Zone, Wuhan (Wuhan Area, Free Trade Zone)

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  • 2-(2-butyl-4-hydroxy-6-MethylpyriMidin-5-yl)-N,N-diMethylacetaMide

  • Casno:

    1315478-13-7

    2-(2-butyl-4-hydroxy-6-MethylpyriMidin-5-yl)-N,N-diMethylacetaMide

    Min.Order: 0

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    factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

    Henan Kanbei Chemical Co., Ltd. is a modern high-tech chemical enterprise integrating R&D, production and sales. The company has strong technical strength, advanced equipment, stri

  •  Henan Kanbei Chemical Co.,LTD

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-152-37804566

    Address:Evergrande Future City, intersection of Zhengkai Avenue and Sixteenth Street, Kaifeng Area, Henan Pilot Free Trade Zone

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  • 2-(2-butyl-4-methyl-6-oxo-1,6-dihydropyrimidin-5-yl)-N,N-dimethylacetamide

  • Casno:

    1315478-13-7

    2-(2-butyl-4-methyl-6-oxo-1,6-dihydropyrimidin-5-yl)-N,N-dimethylacetamide

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    We product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Application:Pharm intermediate

    HANGZHOU TIANYE CHEMICALS Co.LTD , Located in Eastern Science and Innovation Park Hangzhou . We are a high-tech enterprise specialized in technical research and development, produc

  •  HANGZHOU TIANYE CHEMICALS CO., LTD.

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:0571-85083592

    Address:1208# HuaCe Building-B,Wuchanggang Road,XIHU District,Hangzhou City,Zhejiang Province ,China

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  • 2-(2-butyl-4-methyl-6-oxo-1,6-dihydropyrimidin-5- yl)-N,N-dimethylacetamide

  • Casno:

    1315478-13-7

    2-(2-butyl-4-methyl-6-oxo-1,6-dihydropyrimidin-5- yl)-N,N-dimethylacetamide

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    2-(2-butyl-4-methyl-6-oxo-1,6-dihydropyrimidin-5- yl)-N,N-dimethylacetamideAppearance:detailed see specifications Storage:Store in dry, dark and ventilated place Package:foil bags, drums or bottles Application:Pharmaceutical Intermediates Transportat

    Hunan Runhui Chem Co., Ltd. is a comprehensive Fine chemicals and Pharmaceuticals Intermediates supplier in China , Established in Changsha City of Hunan province registered capit

  •  Hunan Longxianng Runhui Trading Co.,Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-731-85570686

    Address:29 Floor,Changsheng Upper Strata,Furong District,China

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  • 2-Butyl-1,6-dihydro-N,N,4-trimethyl-6-oxo-5-pyrimidineacetamide

  • Casno:

    1315478-13-7

    2-Butyl-1,6-dihydro-N,N,4-trimethyl-6-oxo-5-pyrimidineacetamide

    Min.Order: 100 Kilogram

    FOB Price:  USD $ 0.0-0.0

    FIMASARTAN INTERMEDIATE Appearance:white powder Application:pharmaceutical Port:Shanghai, China

    Shanghai Sunwise Chemical Co., Ltd facilitates the deliveries of fine and specialty chemicals from China to global markets. We align suppliers and buyers and then take full respons

  • Shanghai Sunwise Chemical Co., Ltd

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-021-33883180

    Address:Room 10E, Building G, Westlink Center, No. 2337 Gudai Road, Minhang District, Shanghai, China PC: 201100

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