CAS No.1484-85-1,HOMOPIPERONYLAMINE Suppliers

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Basic Information

Molecular Structure:
CAS No.:	1484-85-1
Name:	HOMOPIPERONYLAMINE
Article Data:	87

Formula:	C₉H₁₁NO₂
Molecular Weight:	165.192
Synonyms:	Phenethylamine,3,4-(methylenedioxy)- (7CI,8CI);2-(3,4-Methylenedioxyphenyl)ethylamine;2-(Benzo[d][1,3]dioxol-5-yl)ethanamine;2-Benzo[1,3]dioxol-5-yl-ethylamine;2-Benzo[1,3]dioxol-5-ylethanamine;3,4-(Methylenedioxy)-b-phenethylamine;3,4-(Methylenedioxy)phenethylamine;3,4-(Methylenedioxy)phenylethylamine;5-(2-Aminoethyl)benzodioxole;Homopiperonylamine;[2-(Benzodioxol-5-yl)ethyl]amine;
EINECS:	216-060-8
Density:	1.204 g/c³
Melting Point:	114 °C
Boiling Point:	274.3 ºCat 760 mmHg
Flash Point:	129.8 ºC
Appearance:	Colourless Liquid
Hazard Symbols:	Xi
Risk Codes:	41
Safety:	26-39-24/25
PSA:	44.48000
LogP:	1.61680

Synthetic route

: 1485-00-3
5-(2-nitrovinyl)benzo[1,3]dioxole

: 1484-85-1
3,4-methylenedioxyphenylethylamine

Conditions

Conditions	Yield
With lithium aluminium tetrahydride In tetrahydrofuran at 20 - 70℃; for 4h;	100%
With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; for 4h;	95%
With diisobutylaluminium hydride In 1,4-dioxane at 60℃; for 3h;	82%

: 550358-40-2
benzyl N-[2-(benzo[1,3]dioxol-5-yl)ethyl]carbamate

: 1484-85-1
3,4-methylenedioxyphenylethylamine

Conditions

Conditions	Yield
With hydrogen; palladium on activated charcoal In tetrahydrofuran; methanol at 20℃; under 760 Torr; for 3h;	100%

: C9H9NO2

: 1484-85-1
3,4-methylenedioxyphenylethylamine

Conditions

Conditions	Yield
With hydrogen In ethanol at 70℃; under 112511 Torr; for 6h; Green chemistry;	95.6%

: 1485-00-3, 22568-48-5
5-((E)-2-nitroethenyl)-1,3-benzodioxole

: 1484-85-1
3,4-methylenedioxyphenylethylamine

Conditions

Conditions	Yield
With lithium aluminium tetrahydride In tetrahydrofuran; diethyl ether at 0 - 70℃; for 12h; Inert atmosphere;	95%
With lithium aluminium tetrahydride In tetrahydrofuran Reflux;	87%
With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; Reflux;	84%

: 4439-02-5
3,4-methylenedioxyphenylacetonitrile

: 1484-85-1
3,4-methylenedioxyphenylethylamine

Conditions

Conditions	Yield
With lithium aluminium tetrahydride; aluminium trichloride In diethyl ether for 2h;	92%
With diisobutylaluminium hydride In tetrahydrofuran at 60℃; for 3h; Product distribution; other solvent, temp., time, reagent;	80%
With diisobutylaluminium hydride In tetrahydrofuran at 60℃; for 3h;	80%

: 20799-84-2
3-(benzo[d][1,3]dioxol-5-yl)propanamide

: 1484-85-1
3,4-methylenedioxyphenylethylamine

Conditions

Conditions	Yield
With chlorine; sodium hydroxide In water at -5 - 40℃; for 4h; Reagent/catalyst; Temperature;	91%
With chlorine; sodium hydroxide at 30 - 75℃; for 2h; Green chemistry;	90%
With sodium hydroxide; bromine In water at 70 - 80℃; for 0.25h;	71%
With sodium hypochlorite at 70 - 80℃;

: 21473-47-2
5-(2-nitroethyl)benzo[1,3]dioxole

: 1484-85-1
3,4-methylenedioxyphenylethylamine

Conditions

Conditions	Yield
With lithium aluminium tetrahydride	75%
With hydrogenchloride; iron In methanol; water for 0.5h; Heating;	71%
With hydrogenchloride; zinc
With hydrogenchloride; zinc In ethanol; water for 3h;

: 5-(2-nitro-1(Z)-ethenyl)benzo[d][1,3]dioxol

: 1484-85-1
3,4-methylenedioxyphenylethylamine

Conditions

Conditions	Yield
With hydrogenchloride; iron In methanol; water for 0.5h; Heating;	70%

: 153361-93-4
benzo[1,3]dioxol-5-yl-acetaldehyde-oxime

: 1484-85-1
3,4-methylenedioxyphenylethylamine

Conditions

Conditions	Yield
With sodium amalgam; acetic acid
With ethanol; calcium
With ethanol; sodium

: 119798-32-2
α-acetoxy-2-(3,4-methylenedioxyphenyl)acetonitrile

: 1484-85-1
3,4-methylenedioxyphenylethylamine

Conditions

Conditions	Yield
With methanol; palladium; acetic acid Hydrogenation.Zusatz von wenig Salzsaeure;
With sulfuric acid; palladium; acetic acid Hydrogenation;

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Chemistry

The Molecular Structure of 1,3-Benzodioxole-5-ethanamine (CAS NO.1484-85-1):

Empirical Formula: C₉H₁₁NO₂
Molecular Weight: 165.1891
EINECS: 216-060-8
IUPAC Name: 2-(1,3-Benzodioxol-5-yl)ethanamine
Appearance: Colourless Liquid
Product Categories: Pharmaceutical Intermediates; Intermediates
Nominal Mass: 165
Average Mass: 165.1891
Monoisotopic Mass: 165.078979
Index of Refraction: 1.577
Molar Refractivity: 45.49 cm³
Molar Volume: 137.1 cm³
Surface Tension: 52 dyne/cm
Density: 1.204 g/cm³
Flash Point: 129.8 °C
Enthalpy of Vaporization: 51.27 kJ/mol
Boiling Point: 274.3 °C at 760 mmHg
Vapour Pressure: 0.00543 mmHg at 25 °C

Uses

1,3-Benzodioxole-5-ethanamine (CAS NO.1484-85-1) is used as an intermediate in the synthesis of pharmaceutical actives and other fine chemicals.

Toxicity Data With Reference

Organism	Test Type	Route	Reported Dose (Normalized Dose)	Effect	Source
mouse	LDLo	intraperitoneal	300mg/kg (300mg/kg)	BEHAVIORAL: EXCITEMENT LUNGS, THORAX, OR RESPIRATION: RESPIRATORY STIMULATION	Journal of Physiology. Vol. 76, Pg. 224, 1932.

Specification

1,3-Benzodioxole-5-ethanamine (CAS NO.1484-85-1) is called as 2-(3,4-(Methylendioxy)phenyl)ethylamine ; 2-(3',4'-Methylenedioxy-phenyl)ethylamine ; 3,4-mde ; 3,4-Methylenedioxyphenethylamine ; 3,4-(Methylenedioxyphenyl)ethylamine ; Dl-mdea ; Homopiperonylamine .