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CAS No.: | 1512-30-7 |
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Name: | difluoromethanesulphonyl chloride |
Article Data: | 9 |
Molecular Structure: | |
Formula: | CH Cl F2 O2 S |
Molecular Weight: | 150.534 |
Synonyms: | Methanesulfonylchloride, difluoro- (6CI,8CI,9CI); Difluoromethanesulfonyl chloride |
Density: | 1.696g/cm3 |
Boiling Point: | 84.7°Cat760mmHg |
Flash Point: | 5°C |
PSA: | 42.52000 |
LogP: | 1.85840 |
[(difluoromethyl)thio]methylbenzene
difluoromethylsulfonyl chloride
Conditions | Yield |
---|---|
With water; chlorine at -5 - 10℃; for 3h; | 82% |
With water; chlorine at -10℃; Inert atmosphere; | 72% |
With chlorine In water at -10℃; | 72% |
difluoromethanesulfonic acid
difluoromethylsulfonyl chloride
Conditions | Yield |
---|---|
With phosphorus pentachloride |
Conditions | Yield |
---|---|
With tris-(trimethylsilyl)silane; tris[2-phenylpyridinato-C2,N]iridium(III) In acetonitrile at 20℃; Michael Addition; Inert atmosphere; Sealed tube; Irradiation; | 100% |
Conditions | Yield |
---|---|
With dilauryl peroxide In dichloromethane at 70℃; for 8h; Reagent/catalyst; Solvent; Temperature; Inert atmosphere; | 99% |
difluoromethylsulfonyl chloride
N-(4-acetylphenyl)-2-propenamide
Conditions | Yield |
---|---|
With dipotassium hydrogenphosphate; [Cu(2,9-bis(4-methoxyphenyl)-1,10-phenanthroline)2]Cl In 1,2-dichloro-ethane at 100℃; Sealed tube; Inert atmosphere; Irradiation; | 98% |
Conditions | Yield |
---|---|
With dipotassium hydrogenphosphate; [Cu(2,9-bis(4-methoxyphenyl)-1,10-phenanthroline)2]Cl In 1,2-dichloro-ethane at 100℃; Sealed tube; Inert atmosphere; Irradiation; | 98% |
difluoromethylsulfonyl chloride
Conditions | Yield |
---|---|
With tris[2-phenylpyridinato-C2,N]iridium(III); sodium carbonate In 1,4-dioxane; water at 20℃; for 18h; Inert atmosphere; Sealed tube; Photolysis; | 98% |
difluoromethylsulfonyl chloride
Conditions | Yield |
---|---|
With disodium hydrogenphosphate; fac-tris(2-phenylpyridinato-N,C2')iridium(III) In acetonitrile at 20 - 55℃; for 18h; Inert atmosphere; Sealed tube; Irradiation; | 98% |
difluoromethylsulfonyl chloride
N-(4-cyanophenyl)prop-2-enamide
Conditions | Yield |
---|---|
With dipotassium hydrogenphosphate; [Cu(2,9-bis(4-methoxyphenyl)-1,10-phenanthroline)2]Cl In 1,2-dichloro-ethane at 100℃; Sealed tube; Inert atmosphere; Irradiation; | 96% |
Conditions | Yield |
---|---|
With dipotassium hydrogenphosphate; [Cu(2,9-bis(4-methoxyphenyl)-1,10-phenanthroline)2]Cl In 1,2-dichloro-ethane at 100℃; Sealed tube; Inert atmosphere; Irradiation; | 95% |