CAS No.15352-77-9,β-bisabolol,(1S)-1-[(1S)-1,5-dimethyl-4-hexenyl]-4-methyl-3-cyclohexen-1-ol,β-bisabolol Suppliers

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Basic Information

Molecular Structure:
CAS No.:	15352-77-9
Name:	β-bisabolol,(1S)-1-[(1S)-1,5-dimethyl-4-hexenyl]-4-methyl-3-cyclohexen-1-ol,β-bisabolol
Article Data:	1

Formula:	C15H26 O
Molecular Weight:	222.371
Synonyms:	3-Cyclohexen-1-ol,1-(1,5-dimethyl-4-hexenyl)-4-methyl- (8CI); 3-Cyclohexen-1-ol, 1-(1,5-dimethyl-4-hexenyl)-4-methyl-,[S-(R,R)]-; 3-Cyclohexen-1-ol, 1-[(1S)-1,5-dimethyl-4-hexenyl]-4-methyl-,(1S)- (9CI); b-Bisabolol
Density:	0.921g/cm³
Boiling Point:	305.7°Cat760mmHg
Flash Point:	130.5°C
PSA:	20.23000
LogP:	4.23020

Synthetic route

: 105987-39-1
[(S)-1-((S)-1,5-Dimethyl-hex-4-enyl)-4-methyl-cyclohex-3-enyloxy]-trimethyl-silane

: 15352-77-9
(+)-(4S,8S)-β-bisabolol

Conditions

Conditions	Yield
With hydrogenchloride; water In methanol for 1h;

: 73069-45-1
(-)-(S)-p-mentha-1,8-dien-4-ol

: 15352-77-9
(+)-(4S,8S)-β-bisabolol

Conditions

Conditions	Yield
Multi-step reaction with 11 steps 1: CO/H2 / RhH(Co)(PPh3)3 / hexane / 6 h / 110 °C / 150012 Torr 2: LiAlH4 / diethyl ether / 2 h / Heating 3: pyridine / 2 h / Ambient temperature 4: hexamethyldisilazane, pyridine / 48 h / Heating 5: LiAlH4 / diethyl ether / 1 h / Heating 6: PDC, NaOAc / CH2Cl2 / 2 h / Ambient temperature 7: 1.) BuLi / diethyl ether; hexane / 1.) 4 h, RT, 2.) reflux, 5 h 8: 1.) BBN, 2.) 30percent H2O2, 10percent NaOH / 1.) THF, 0 deg C, 5 h, RT, 18h, 2.) H2O, 1 h 9: PDC, NaOAc / CH2Cl2 10: 1.) BuLi / diethyl ether; hexane / 1 h / Heating 11: HCl, H2O / methanol / 1 h View Scheme

Yield

Multi-step reaction with 11 steps
1: CO/H2 / RhH(Co)(PPh3)3 / hexane / 6 h / 110 °C / 150012 Torr
2: LiAlH4 / diethyl ether / 2 h / Heating
3: pyridine / 2 h / Ambient temperature
4: hexamethyldisilazane, pyridine / 48 h / Heating
5: LiAlH4 / diethyl ether / 1 h / Heating
6: PDC, NaOAc / CH2Cl2 / 2 h / Ambient temperature
7: 1.) BuLi / diethyl ether; hexane / 1.) 4 h, RT, 2.) reflux, 5 h
8: 1.) BBN, 2.) 30percent H2O2, 10percent NaOH / 1.) THF, 0 deg C, 5 h, RT, 18h, 2.) H2O, 1 h
9: PDC, NaOAc / CH2Cl2
10: 1.) BuLi / diethyl ether; hexane / 1 h / Heating
11: HCl, H2O / methanol / 1 h
View Scheme

: 106035-80-7
(1R,3S,6S)-3-Isopropenyl-6-methyl-7-oxa-bicyclo[4.1.0]heptan-3-ol

: 15352-77-9
(+)-(4S,8S)-β-bisabolol

Conditions

Conditions	Yield
Multi-step reaction with 12 steps 1: Zn dust, NaOAc, NaI / acetic acid / 25 h 2: CO/H2 / RhH(Co)(PPh3)3 / hexane / 6 h / 110 °C / 150012 Torr 3: LiAlH4 / diethyl ether / 2 h / Heating 4: pyridine / 2 h / Ambient temperature 5: hexamethyldisilazane, pyridine / 48 h / Heating 6: LiAlH4 / diethyl ether / 1 h / Heating 7: PDC, NaOAc / CH2Cl2 / 2 h / Ambient temperature 8: 1.) BuLi / diethyl ether; hexane / 1.) 4 h, RT, 2.) reflux, 5 h 9: 1.) BBN, 2.) 30percent H2O2, 10percent NaOH / 1.) THF, 0 deg C, 5 h, RT, 18h, 2.) H2O, 1 h 10: PDC, NaOAc / CH2Cl2 11: 1.) BuLi / diethyl ether; hexane / 1 h / Heating 12: HCl, H2O / methanol / 1 h View Scheme

Yield

Multi-step reaction with 12 steps
1: Zn dust, NaOAc, NaI / acetic acid / 25 h
2: CO/H2 / RhH(Co)(PPh3)3 / hexane / 6 h / 110 °C / 150012 Torr
3: LiAlH4 / diethyl ether / 2 h / Heating
4: pyridine / 2 h / Ambient temperature
5: hexamethyldisilazane, pyridine / 48 h / Heating
6: LiAlH4 / diethyl ether / 1 h / Heating
7: PDC, NaOAc / CH2Cl2 / 2 h / Ambient temperature
8: 1.) BuLi / diethyl ether; hexane / 1.) 4 h, RT, 2.) reflux, 5 h
9: 1.) BBN, 2.) 30percent H2O2, 10percent NaOH / 1.) THF, 0 deg C, 5 h, RT, 18h, 2.) H2O, 1 h
10: PDC, NaOAc / CH2Cl2
11: 1.) BuLi / diethyl ether; hexane / 1 h / Heating
12: HCl, H2O / methanol / 1 h
View Scheme

: 3-((S)-1-Hydroxy-4-methyl-cyclohex-3-enyl)-butyraldehyde

: 15352-77-9
(+)-(4S,8S)-β-bisabolol

Conditions

Conditions	Yield
Multi-step reaction with 10 steps 1: LiAlH4 / diethyl ether / 2 h / Heating 2: pyridine / 2 h / Ambient temperature 3: hexamethyldisilazane, pyridine / 48 h / Heating 4: LiAlH4 / diethyl ether / 1 h / Heating 5: PDC, NaOAc / CH2Cl2 / 2 h / Ambient temperature 6: 1.) BuLi / diethyl ether; hexane / 1.) 4 h, RT, 2.) reflux, 5 h 7: 1.) BBN, 2.) 30percent H2O2, 10percent NaOH / 1.) THF, 0 deg C, 5 h, RT, 18h, 2.) H2O, 1 h 8: PDC, NaOAc / CH2Cl2 9: 1.) BuLi / diethyl ether; hexane / 1 h / Heating 10: HCl, H2O / methanol / 1 h View Scheme

Yield

Multi-step reaction with 10 steps
1: LiAlH4 / diethyl ether / 2 h / Heating
2: pyridine / 2 h / Ambient temperature
3: hexamethyldisilazane, pyridine / 48 h / Heating
4: LiAlH4 / diethyl ether / 1 h / Heating
5: PDC, NaOAc / CH2Cl2 / 2 h / Ambient temperature
6: 1.) BuLi / diethyl ether; hexane / 1.) 4 h, RT, 2.) reflux, 5 h
7: 1.) BBN, 2.) 30percent H2O2, 10percent NaOH / 1.) THF, 0 deg C, 5 h, RT, 18h, 2.) H2O, 1 h
8: PDC, NaOAc / CH2Cl2
9: 1.) BuLi / diethyl ether; hexane / 1 h / Heating
10: HCl, H2O / methanol / 1 h
View Scheme

: 3-<(1S)-1-hydroxy-4-methylcyclohex-3-enyl>butanol

: 15352-77-9
(+)-(4S,8S)-β-bisabolol

Conditions

Conditions	Yield
Multi-step reaction with 9 steps 1: pyridine / 2 h / Ambient temperature 2: hexamethyldisilazane, pyridine / 48 h / Heating 3: LiAlH4 / diethyl ether / 1 h / Heating 4: PDC, NaOAc / CH2Cl2 / 2 h / Ambient temperature 5: 1.) BuLi / diethyl ether; hexane / 1.) 4 h, RT, 2.) reflux, 5 h 6: 1.) BBN, 2.) 30percent H2O2, 10percent NaOH / 1.) THF, 0 deg C, 5 h, RT, 18h, 2.) H2O, 1 h 7: PDC, NaOAc / CH2Cl2 8: 1.) BuLi / diethyl ether; hexane / 1 h / Heating 9: HCl, H2O / methanol / 1 h View Scheme

Yield

Multi-step reaction with 9 steps
1: pyridine / 2 h / Ambient temperature
2: hexamethyldisilazane, pyridine / 48 h / Heating
3: LiAlH4 / diethyl ether / 1 h / Heating
4: PDC, NaOAc / CH2Cl2 / 2 h / Ambient temperature
5: 1.) BuLi / diethyl ether; hexane / 1.) 4 h, RT, 2.) reflux, 5 h
6: 1.) BBN, 2.) 30percent H2O2, 10percent NaOH / 1.) THF, 0 deg C, 5 h, RT, 18h, 2.) H2O, 1 h
7: PDC, NaOAc / CH2Cl2
8: 1.) BuLi / diethyl ether; hexane / 1 h / Heating
9: HCl, H2O / methanol / 1 h
View Scheme

: 3-<(1S)-4-methyl-1-(trimethylsilyloxy)cyclohex-3-enyl>butyl acetate

: 15352-77-9
(+)-(4S,8S)-β-bisabolol

Conditions

Conditions	Yield
Multi-step reaction with 7 steps 1: LiAlH4 / diethyl ether / 1 h / Heating 2: PDC, NaOAc / CH2Cl2 / 2 h / Ambient temperature 3: 1.) BuLi / diethyl ether; hexane / 1.) 4 h, RT, 2.) reflux, 5 h 4: 1.) BBN, 2.) 30percent H2O2, 10percent NaOH / 1.) THF, 0 deg C, 5 h, RT, 18h, 2.) H2O, 1 h 5: PDC, NaOAc / CH2Cl2 6: 1.) BuLi / diethyl ether; hexane / 1 h / Heating 7: HCl, H2O / methanol / 1 h View Scheme

Yield

Multi-step reaction with 7 steps
1: LiAlH4 / diethyl ether / 1 h / Heating
2: PDC, NaOAc / CH2Cl2 / 2 h / Ambient temperature
3: 1.) BuLi / diethyl ether; hexane / 1.) 4 h, RT, 2.) reflux, 5 h
4: 1.) BBN, 2.) 30percent H2O2, 10percent NaOH / 1.) THF, 0 deg C, 5 h, RT, 18h, 2.) H2O, 1 h
5: PDC, NaOAc / CH2Cl2
6: 1.) BuLi / diethyl ether; hexane / 1 h / Heating
7: HCl, H2O / methanol / 1 h
View Scheme

: 105987-22-2
(S)-3-((S)-4-Methyl-1-trimethylsilanyloxy-cyclohex-3-enyl)-butan-1-ol

: 15352-77-9
(+)-(4S,8S)-β-bisabolol

Conditions

Conditions	Yield
Multi-step reaction with 6 steps 1: PDC, NaOAc / CH2Cl2 / 2 h / Ambient temperature 2: 1.) BuLi / diethyl ether; hexane / 1.) 4 h, RT, 2.) reflux, 5 h 3: 1.) BBN, 2.) 30percent H2O2, 10percent NaOH / 1.) THF, 0 deg C, 5 h, RT, 18h, 2.) H2O, 1 h 4: PDC, NaOAc / CH2Cl2 5: 1.) BuLi / diethyl ether; hexane / 1 h / Heating 6: HCl, H2O / methanol / 1 h View Scheme

: Acetic acid 3-((S)-1-hydroxy-4-methyl-cyclohex-3-enyl)-butyl ester

: 15352-77-9
(+)-(4S,8S)-β-bisabolol

Conditions

Conditions	Yield
Multi-step reaction with 8 steps 1: hexamethyldisilazane, pyridine / 48 h / Heating 2: LiAlH4 / diethyl ether / 1 h / Heating 3: PDC, NaOAc / CH2Cl2 / 2 h / Ambient temperature 4: 1.) BuLi / diethyl ether; hexane / 1.) 4 h, RT, 2.) reflux, 5 h 5: 1.) BBN, 2.) 30percent H2O2, 10percent NaOH / 1.) THF, 0 deg C, 5 h, RT, 18h, 2.) H2O, 1 h 6: PDC, NaOAc / CH2Cl2 7: 1.) BuLi / diethyl ether; hexane / 1 h / Heating 8: HCl, H2O / methanol / 1 h View Scheme

Yield

Multi-step reaction with 8 steps
1: hexamethyldisilazane, pyridine / 48 h / Heating
2: LiAlH4 / diethyl ether / 1 h / Heating
3: PDC, NaOAc / CH2Cl2 / 2 h / Ambient temperature
4: 1.) BuLi / diethyl ether; hexane / 1.) 4 h, RT, 2.) reflux, 5 h
5: 1.) BBN, 2.) 30percent H2O2, 10percent NaOH / 1.) THF, 0 deg C, 5 h, RT, 18h, 2.) H2O, 1 h
6: PDC, NaOAc / CH2Cl2
7: 1.) BuLi / diethyl ether; hexane / 1 h / Heating
8: HCl, H2O / methanol / 1 h
View Scheme

: 105987-36-8
Trimethyl-[(S)-4-methyl-1-((S)-1-methyl-but-3-enyl)-cyclohex-3-enyloxy]-silane

: 15352-77-9
(+)-(4S,8S)-β-bisabolol

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: 1.) BBN, 2.) 30percent H2O2, 10percent NaOH / 1.) THF, 0 deg C, 5 h, RT, 18h, 2.) H2O, 1 h 2: PDC, NaOAc / CH2Cl2 3: 1.) BuLi / diethyl ether; hexane / 1 h / Heating 4: HCl, H2O / methanol / 1 h View Scheme

: 105987-37-9
(S)-4-((S)-4-Methyl-1-trimethylsilanyloxy-cyclohex-3-enyl)-pentan-1-ol

: 15352-77-9
(+)-(4S,8S)-β-bisabolol

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: PDC, NaOAc / CH2Cl2 2: 1.) BuLi / diethyl ether; hexane / 1 h / Heating 3: HCl, H2O / methanol / 1 h View Scheme

Casno:
15352-77-9
beta-bisabolol
Min.Order: 1 Kilogram
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Casno:
15352-77-9
β-bisabolol,(1S)-1-[(1S)-1,5-dimethyl-4-hexenyl]-4-methyl-3-cyclohexen-1-ol,β-bisabolol CAS 15352-77-9
Min.Order: 1 Kilogram
FOB Price: USD $ 1.0-10.0
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Casno:
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3-Cyclohexen-1-ol,1-[(1S)-1,5-dimethyl-4-hexen-1-yl]-4-methyl-, (1S)-
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Casno:
15352-77-9
β-bisabolol,(1S)-1-[(1S)-1,5-dimethyl-4-hexenyl]-4-methyl-3-cyclohexen-1-ol,β-bisabolol
Min.Order: 1 Kilogram
FOB Price: USD $ 2.0-2.0
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beta-Bisabolol
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尾-bisabolol,(1S)-1-[(1S)-1,5-dimethyl-4-hexenyl]-4-methyl-3-cyclohexen-1-ol,尾-bisabolol
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3-Cyclohexen-1-ol,1-[(1S)-1,5-dimethyl-4-hexen-1-yl]-4-methyl-, (1S)-
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