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CAS No.: | 1580-20-7 |
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Name: | 1,2,3,4,5,6,7,8,9,10-decafluorophenanthrene |
Article Data: | 5 |
Molecular Structure: | |
Formula: | C14F10 |
Molecular Weight: | 358.138 |
Synonyms: | Phenanthrene,decafluoro- (7CI,8CI,9CI); Decafluorophenanthrene; Perfluorophenanthrene |
Density: | 1.792g/cm3 |
Boiling Point: | 356.6°Cat760mmHg |
Flash Point: | 123.8°C |
PSA: | 0.00000 |
LogP: | 5.38400 |
Conditions | Yield |
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With bis(cyclopentadienyl)titanium dichloride; iodine; aluminium; mercury dichloride In tetrahydrofuran Schlenk technique; Inert atmosphere; | 28% |
With benzophenone; sodium In tetrahydrofuran for 1.5h; -70 deg C to rt; | 22% |
With titanocene difluoride; aluminium; mercury dichloride In tetrahydrofuran for 24h; Ambient temperature; |
Conditions | Yield |
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(i) KCoF4, (heating), (ii) Fe2O3, (thermolysis); Multistep reaction; |
Conditions | Yield |
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With fuming sulphuric acid at 100℃; for 3h; Schlenk technique; Inert atmosphere; | 33% |
Conditions | Yield |
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In methanol |
decafluorophenanthrene
2,2'-octafluorodiphenic Acid
Conditions | Yield |
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With potassium permanganate In acetone |
decafluorophenanthrene
dimethyl amine
2,7-Bis-dimethylamino-octafluorphenanthren
Conditions | Yield |
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In ethanol |
decafluorophenanthrene
3,5,6,3',5',6'-Hexafluoro-4,4'-dimethoxy-biphenyl-2,2'-dicarboxylic acid
Conditions | Yield |
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Multi-step reaction with 2 steps 1: methanol 2: KMnO4 / acetone View Scheme |
Conditions | Yield |
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In not given crystn.; |
bis(pentamethylcyclopentadienyl)iron(II)
decafluorophenanthrene
decamethylferrocene * perfluorophenanthrene
Conditions | Yield |
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In pentane equimolar amts.; crystn. on slow evapn. (2 d); |