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160199-05-3

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Basic Information
CAS No.: 160199-05-3
Name: 2,4-dichloro-benzo[4,5]thieno[3,2-d]pyrimidine
Article Data: 12
Molecular Structure:
Molecular Structure of 160199-05-3 (2,4-dichloro-benzo[4,5]thieno[3,2-d]pyrimidine)
Formula: C10H4Cl2N2S
Molecular Weight: 255.127
Synonyms: 2,4-dichloro-benzo[4,5]thieno[3,2-d]pyrimidine;2,4-dichlorobenzo[4,5]thieno[3,2-d]pyridine;2,4-Dichloro-[1]benzothieno[3,2-d]pyrimidine
Density: 1.619±0.06 g/cm3(Predicted)
PSA: 54.02000
LogP: 4.15130
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Synthetic route
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(benzo-1H-thieno[3,2-d]pyrimidine-2,4-dione)

160199-05-3

2,4-dichlorobenzo[4,5]thiophene[3,2-d]pyrimidine

Conditions
ConditionsYield
With trichlorophosphate85%
With trichlorophosphate for 6h; Reflux;85%
With trichlorophosphate for 6h; Reflux;85%
394-47-8

2-fluorobenzonitrile

160199-05-3

2,4-dichlorobenzo[4,5]thiophene[3,2-d]pyrimidine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: potassium tert-butylate / N,N-dimethyl-formamide
2: 2 h / 200 °C
3: trichlorophosphate
View Scheme
35212-85-2

3-Amino-benzo[b]thiophene-2-carboxylic acid methyl ester

160199-05-3

2,4-dichlorobenzo[4,5]thiophene[3,2-d]pyrimidine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 2 h / 200 °C
2: trichlorophosphate
View Scheme
Multi-step reaction with 2 steps
1: 2 h / 200 °C
2: trichlorophosphate / 6 h / Reflux
View Scheme
Multi-step reaction with 2 steps
1: 2 h / 200 °C
2: trichlorophosphate / 8 h / Reflux
View Scheme
Multi-step reaction with 2 steps
1: 2 h / 200 °C
2: trichlorophosphate / 7.5 h / Reflux
View Scheme
611-20-1

salicylonitrile

160199-05-3

2,4-dichlorobenzo[4,5]thiophene[3,2-d]pyrimidine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: triethylamine / dimethyl sulfoxide / 3 h / 100 °C
2: 2 h / 200 °C
3: trichlorophosphate / 6 h / Reflux
View Scheme
160199-05-3

2,4-dichlorobenzo[4,5]thiophene[3,2-d]pyrimidine

1257220-47-5

12,12-dimethyl-10,12-dihydro-10-azaindeno[2,1-b]fluorene

C31H20ClN3S

Conditions
ConditionsYield
With bis(tri-t-butylphosphine)palladium(0); sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene for 4h; Reflux;90%
160199-05-3

2,4-dichlorobenzo[4,5]thiophene[3,2-d]pyrimidine

2-(4-(4,4,5,5-tetramethyl-[1,3,2]-dioxaborolan-2-yl)phenyl)-4,6-diphenylpyrimidine

C32H19ClN4S

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water for 9h; Inert atmosphere; Heating;85%
160199-05-3

2,4-dichlorobenzo[4,5]thiophene[3,2-d]pyrimidine

98-80-6

phenylboronic acid

4-chloro-6-phenyl-8-thia-3,5-diazatricyclo[7.4.0.0,]trideca-1(13),2,4,6,9,11-hexaene

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water for 7h; Inert atmosphere; Heating;83%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water for 9h; Inert atmosphere; Heating;83%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water for 7h; Heating;83%
160199-05-3

2,4-dichlorobenzo[4,5]thiophene[3,2-d]pyrimidine

2,4-diphenyl-6-(4-(4,4',5,5'-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-1,3,5-triazine

C31H18ClN5S

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water for 9h; Inert atmosphere; Heating;81%
854952-58-2

N-phenyl-9H-carbazol-3-boronic acid

160199-05-3

2,4-dichlorobenzo[4,5]thiophene[3,2-d]pyrimidine

C28H16ClN3S

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); sodium hydroxide In tetrahydrofuran; water at 80℃;80%
160199-05-3

2,4-dichlorobenzo[4,5]thiophene[3,2-d]pyrimidine

1001911-63-2

(9‐phenyl‐9H‐carbazol‐2‐yl)boronic acid

2-chloro-4-(9-phenyl-9H-carbazol-2-yl)benzo[4,5]thieno[3,2-d]pyrimidine

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); sodium hydroxide In 1,4-dioxane; water at 80℃;78%
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