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161552-03-0

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Basic Information
CAS No.: 161552-03-0
Name: CYCLO (ARG-GLY-ASP-D-PHE-LYS)
Article Data: 14
Molecular Structure:
Molecular Structure of 161552-03-0 (CYCLO (ARG-GLY-ASP-D-PHE-LYS))
Formula: C27H41N9O7
Molecular Weight: 603.679
Synonyms: cyclo(Arg-Gly-Asp-d-Phe-Lys)
Density: 1.47±0.1 g/cm3(Predicted)
Melting Point: 191℃ (decomposition)
PSA: 288.17000
LogP: 0.43580
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Synthetic route

C42H51ClN10O11

161552-03-0

[(2S,5R,8S,11S)-8-(4-Amino-butyl)-5-benzyl-11-(3-guanidino-propyl)-3,6,9,12,15-pentaoxo-1,4,7,10,13-pentaaza-cyclopentadec-2-yl]-acetic acid

Conditions
ConditionsYield
With palladium 10% on activated carbon; hydrogen In methanol; acetic acid at 20℃; for 18h;100%

Fmoc-Asp(OAll)-Pol

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N-(fluoren-9-ylmethoxycarbonyl)glycine

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Fmoc-D-Phe-OH

Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine

161552-03-0

[(2S,5R,8S,11S)-8-(4-Amino-butyl)-5-benzyl-11-(3-guanidino-propyl)-3,6,9,12,15-pentaoxo-1,4,7,10,13-pentaaza-cyclopentadec-2-yl]-acetic acid

Conditions
ConditionsYield
Stage #1: Fmoc-Asp(OAll)-Pol
Stage #2: N-(fluoren-9-ylmethoxycarbonyl)glycine
Stage #3: Fmoc-Lys(tert-butoxycarbonyl); Fmoc-D-Phe-OH; Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine Further stages;		43%
...Expand

2-chlorotrityl resin

Fmoc-dPhe-OH

71989-14-5

Fmoc-(tBu)Asp-OH

111061-54-2

Nα-Fmoc-Nε-Trt-Lys

Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine

161552-03-0

[(2S,5R,8S,11S)-8-(4-Amino-butyl)-5-benzyl-11-(3-guanidino-propyl)-3,6,9,12,15-pentaoxo-1,4,7,10,13-pentaaza-cyclopentadec-2-yl]-acetic acid

Conditions
ConditionsYield
Stage #1: H-Gly-(2-Cl)-Trt-pol; Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine With N-ethyl-N,N-diisopropylamine; [ethyl cyano(hydroxyimino)acetato-O2]tri-1-pyrrolidinylphosphonium hexafluorophosphate at 20℃; for 1h; 2-CT Cl resin;
Stage #2: With piperidine In N,N-dimethyl-formamide at 20℃; for 0.1h;
Stage #3: Fmoc-dPhe-OH; Fmoc-(tBu)Asp-OH; Nα-Fmoc-Nε-Trt-Lys Further stages;		43%
...Expand

2-chlorotrityl resin

Fmoc-dPhe-OH

71989-14-5

Fmoc-(tBu)Asp-OH

159766-56-0

Fmoc-Lys(OAc)-OH

Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine

161552-03-0

[(2S,5R,8S,11S)-8-(4-Amino-butyl)-5-benzyl-11-(3-guanidino-propyl)-3,6,9,12,15-pentaoxo-1,4,7,10,13-pentaaza-cyclopentadec-2-yl]-acetic acid

Conditions
ConditionsYield
Stage #1: H-Gly-(2-Cl)-Trt-pol; Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine With N-ethyl-N,N-diisopropylamine; [ethyl cyano(hydroxyimino)acetato-O2]tri-1-pyrrolidinylphosphonium hexafluorophosphate at 20℃; for 1h; 2-CT Cl resin;
Stage #2: With piperidine In N,N-dimethyl-formamide at 20℃; for 0.1h;
Stage #3: Fmoc-dPhe-OH; Fmoc-(tBu)Asp-OH; Fmoc-Lys(OAc)-OH Further stages;		43%
...Expand
388633-54-3

C45H67N9O10S

161552-03-0

[(2S,5R,8S,11S)-8-(4-Amino-butyl)-5-benzyl-11-(3-guanidino-propyl)-3,6,9,12,15-pentaoxo-1,4,7,10,13-pentaaza-cyclopentadec-2-yl]-acetic acid

Conditions
ConditionsYield
With chlorotriisopropylsilane; water; trifluoroacetic acid for 2h;
71989-14-5

Fmoc-(tBu)Asp-OH

86123-10-6

Fmoc-D-Phe-OH

186350-56-1

Alloc-L-Lys(N-Fmoc)-OH

R(Pmc)-G linear peptide bound to resin

R(Pmc)-G linear peptide bound to resin

161552-03-0

[(2S,5R,8S,11S)-8-(4-Amino-butyl)-5-benzyl-11-(3-guanidino-propyl)-3,6,9,12,15-pentaoxo-1,4,7,10,13-pentaaza-cyclopentadec-2-yl]-acetic acid

Conditions
ConditionsYield
Multistep reaction;
...Expand
71989-14-5

Fmoc-(tBu)Asp-OH

Fmoc-Asn-OHFmoc-Leu-OH

Fmoc-Asn-OHFmoc-Leu-OH

161552-03-0

[(2S,5R,8S,11S)-8-(4-Amino-butyl)-5-benzyl-11-(3-guanidino-propyl)-3,6,9,12,15-pentaoxo-1,4,7,10,13-pentaaza-cyclopentadec-2-yl]-acetic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: Pd(PPh3)4; PhSiH3
2: TFA; triisopropylsilane; water / 2 h
View Scheme
86123-10-6

Fmoc-D-Phe-OH

bis-1,4-aminomethylcyclohexane on chlorotrityl resin

bis-1,4-aminomethylcyclohexane on chlorotrityl resin

161552-03-0

[(2S,5R,8S,11S)-8-(4-Amino-butyl)-5-benzyl-11-(3-guanidino-propyl)-3,6,9,12,15-pentaoxo-1,4,7,10,13-pentaaza-cyclopentadec-2-yl]-acetic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: Pd(PPh3)4; PhSiH3
2: TFA; triisopropylsilane; water / 2 h
View Scheme
146982-27-6

(S)-6-allyloxycarbonylamino-2-(9H-fluoren-9-ylmethoxycarbonylamino)-hexanoic acid

161552-03-0

[(2S,5R,8S,11S)-8-(4-Amino-butyl)-5-benzyl-11-(3-guanidino-propyl)-3,6,9,12,15-pentaoxo-1,4,7,10,13-pentaaza-cyclopentadec-2-yl]-acetic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: Pd(PPh3)4; PhSiH3
2: TFA; triisopropylsilane; water / 2 h
View Scheme
343312-39-0

cyclo(-D(tBu)-f-K(Aloc)-R(Pmc)-G-)

161552-03-0

[(2S,5R,8S,11S)-8-(4-Amino-butyl)-5-benzyl-11-(3-guanidino-propyl)-3,6,9,12,15-pentaoxo-1,4,7,10,13-pentaaza-cyclopentadec-2-yl]-acetic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Pd(PPh3)4; PhSiH3
2: TFA; triisopropylsilane; water / 2 h
View Scheme
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    Tel:+86-592-583819

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    c(RGDfK)

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    Business Type:Manufacturers

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    J&H CHEM is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other Value-added customer services, for diversified range products of chemicals

    J&H Chemical is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    CYCLO (ARG-GLY-ASP-D-PHE-LYS)

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    1. Product advantages? High purity, all above 98.5%, no impurities after dissolution? We will test each batch to ensure quality? OEM and private brand services designed for free? Various cap colors available? We can also provide MT1 peptide powder2.

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    Business Type:Lab/Research institutions

    Tel:+86-13437180835

    Address:Experimental Building 311-15, Nuclear Magnetic Spectrometer Industry Base, No. 128 Guanggu 7th Road, Donghu New Technology Development Zone, Wuhan (Wuhan Area, Free Trade Zone)

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    best seller Application:API

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    Business Type:Trading Company

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    Address:No.99 Road, Xi'an, China

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    161552-03-0

    CYCLO (ARG-GLY-ASP-D-PHE-LYS)

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    Henan Kanbei Chemical Co., Ltd. is a modern high-tech chemical enterprise integrating R&D, production and sales. The company has strong technical strength, advanced equipment, stri

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    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-152-37804566

    Address:Evergrande Future City, intersection of Zhengkai Avenue and Sixteenth Street, Kaifeng Area, Henan Pilot Free Trade Zone

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    161552-03-0

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    161552-03-0

    Cyclo(-Arg-Gly-Asp-D-Phe-Lys)

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    Shanghai Yuanye Bio-Technology Co., Ltd. is a comprehensive enterprise of life science, specializing in the research, development and sales of biochemical reagents, analytical stan

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    China (Mainland)  |  Contact Details

    Business Type:Trading Company

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  • Casno:

    161552-03-0

    161552-03-0

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    Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen

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    China (Mainland)  |  Contact Details

    Business Type:Trading Company

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  • Cyclo (-RGDfK)

  • Casno:

    161552-03-0

    Cyclo (-RGDfK)

    Min.Order: 0

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    Cyclo (-RGDfK)Appearance:Solid powder Storage:3 years -20℃powder;6 months-80℃in solvent Application:Inhibitor

    KONING PHARMCHEM CO., LTD. has committed itself to a strategy of providing a unique service for companies involved in the manufacture of pharmaceuticals, healthcare products, food,

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    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-574-87369228

    Address:Lingqiao Road

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