Detail of "1707-77-3"

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CAS Number:
1707-77-3
Name:
D-Mannitol,1,2:5,6-bis-O-(1-methylethylidene)-
Superlist Name:
1,2:5,6-Bis-O-(1-methylethylidene)-D-mannitol
Molecular Structure:
Formula:
C₁₂H₂₂O₆
Molecular Weight:
262.30
Synonyms:
Mannitol,1,2:5,6-di-O-isopropylidene-, D- (8CI);1,2:5,6-Di-O-isopropylidene-D-mannitol;1,2:5,6-Diisopropylidene-D-mannitol;D-(+)-1,2:5,6-Di-O-isopropylidenemannitol;D-Mannitol 1,2:5,6-bis-acetonide;
EINECS:
216-954-8
Density:
1.175 g/cm³
Melting Point:
120-122 °C(lit.)
Boiling Point:
382 °C at 760 mmHg
Flash Point:
184.8 °C
Hazard Symbols:
Xi
Risk Codes:
36/37/38
Safety:
22-24/25-36/37-26 Details

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Reference

Preparation and reaction of cyclic oxalates of diols: Preparation and reaction of cyclic oxalates of diols.Some chemicals with cas registry numbers like 1460-57-7 and 1707-77-3 are also used. Kim, Kwan Soo; Hurh, Eun Young; Na, Kyutae; Chung, Dai Il (Dep. Chem., Yonsei Univ., Seoul 120-749, S. Korea). Synth. Commun., 21(22), 2361-7 (English) 1991. CODEN: SYNCAV. ISSN: 0039-7911. DOCUMENT TYPE: Journal CA Section: 33 (Carbohydrates) Cyclic oxalates, e.g., I, were efficiently prepd. by the reaction of diols with EtO2CCOCl in the presence of NEt3. They were stable under acidic conditions but cleaved to diols under basic conditions. .

Asymmetric reduction of acetophenone by lithium aluminum hydride modified with chiral 1,2,5,6-diisopropylidenemannitol and achiral alcohol or phenol: Asymmetric reduction of acetophenone by lithium aluminum hydride modified with chiral 1,2,5,6-diisopropylidenemannitol and achiral alcohol or phenol. Song, Mingrui; Yan, Liushui; Yin, Chenglie (Dep. Chem., Beijing Normal Univ., Beijing, Peop. Rep. China). Beijing Shifan Daxue Xuebao, Ziran Kexueban, (2), 44-7 (Chinese) 1986. 1707-77-3 and 64-17-5 which are cas registry numbers are also used here. CODEN: BSDKDH. DOCUMENT TYPE: Journal CA Section: 22 (Physical Organic Chemistry) Section cross-reference(s): 25 Chiral complexes formed from 1,2,5,6-diisopropylidenemannitol-lithium aluminum hydride and an alc. and phenol were used for the asym. redn. of acetophenone. In all cases studied R-(+)-phenylmethylcarbinol was produced in excess and the optical yields increased with increasing size of the alkyl group in the alc. used. .

Detail of "1707-77-3"

D-Mannitol,1,2:5,6-bis-O-(1-methylethylidene)-

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CAS No.1707-77-3 1,2:5,6-Bis-O-(1-methylethylidene)-D-mannitol

Reference