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CAS No.: | 18523-47-2 |
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Name: | 3-azidopropanoic acid |
Article Data: | 49 |
Molecular Structure: | |
Formula: | C3H5N3O2 |
Molecular Weight: | 115.092 |
Synonyms: | 3-azido-propionic acid;3-azidopropionic acid;3-Azidopropanoic acid;azidopropionic acid;2-azidopropionic acid; |
PSA: | 87.05000 |
LogP: | 0.22416 |
3-Bromopropionic acid
3-azidopropanoic acid
Conditions | Yield |
---|---|
With sodium azide In water | 100% |
With sodium azide In acetonitrile at 85℃; for 5h; | 90% |
With sodium azide In N,N-dimethyl-formamide for 4h; Reflux; | 89% |
acrylic acid
3-azidopropanoic acid
Conditions | Yield |
---|---|
With trimethylsilylazide In neat (no solvent) at 60℃; for 0.5h; | 99% |
With trimethylsilylazide In water at 60℃; for 0.5h; Reagent/catalyst; Flow reactor; Green chemistry; | 99% |
With trimethylsilylazide; Amberlite IRA900F at 30℃; for 2h; Michael addition; neat (no solvent); | 73% |
chloropropionic acid
3-azidopropanoic acid
Conditions | Yield |
---|---|
With sodium azide In water for 15h; | 85% |
With sodium azide In water at 100℃; for 22h; | 81% |
With sodium azide In water at 85℃; for 12h; | 73% |
With sodium azide In water at 20℃; for 168h; |
β-Propiolactone
3-azidopropanoic acid
Conditions | Yield |
---|---|
With sodium azide In water at 20℃; for 6h; Inert atmosphere; | 15% |
With sodium azide In water at 20℃; for 6h; | 15% |
With sodium azide |
3-azidopropanoic acid
Conditions | Yield |
---|---|
With sulfuric acid |
azido-b-alanine methyl ester
3-azidopropanoic acid
Conditions | Yield |
---|---|
With methanol; lithium hydroxide at 20℃; | |
With sodium hydroxide In methanol at 20℃; for 48h; |
3-amino propanoic acid
3-azidopropanoic acid
Conditions | Yield |
---|---|
With imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; potassium carbonate In methanol at 20℃; for 16h; |
3-azidopropionic acid ethyl ester
3-azidopropanoic acid
Conditions | Yield |
---|---|
With sodium hydroxide In methanol Inert atmosphere; |
3-azidopropanoic acid
3-azidopropionyl chloride
Conditions | Yield |
---|---|
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 0 - 20℃; | 100% |
With oxalyl dichloride In dichloromethane at 20℃; for 6h; | |
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane for 3h; | |
With oxalyl dichloride In dichloromethane for 6h; | |
With thionyl chloride In dichloromethane at 20℃; for 12h; |
3-azidopropanoic acid
phenylacetylene
3-(4-phenyl-1H-[1,2,3]triazol-1-yl)-propionic acid
Conditions | Yield |
---|---|
With copper(II) acetate monohydrate; triethylamine In water; acetonitrile at 20℃; for 8h; | 100% |
With copper(ll) sulfate pentahydrate; sodium L-ascorbate In water; tert-butyl alcohol at 20℃; for 12h; | 46% |