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253128-41-5

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Basic Information
CAS No.: 253128-41-5
Name: Eribulin
Article Data: 11
Molecular Structure:
Molecular Structure of 253128-41-5 (Eribulin)
Formula: C40H59NO11
Molecular Weight: 729.909
Synonyms: B 1939;E 7389;ER 086526;Eribulin;
EINECS: 803-583-7
Density: 1.29±0.1 g/cm3(Predicted)
PSA: 146.39000
LogP: 4.13830
Related products
Synthetic route

C40H61NO12

253128-41-5

(1S,3S,6S,9S,12S,14R,16R,18S,20R,21R,22S,26R,29S,31R,32S,33R,35R,36S)-20-[(2S)-3-Amino-2-hydroxypropyl]-21-methoxy-14-methyl-8,15-bis(methylene)-2,19,30,34,37,39,40,41-octaoxanonacyclo [24.9.2.13,32.13,33.16,9.112,16.018,22.029,36.031,35]hentetracontan-24-one

Conditions
ConditionsYield
With pyridinium p-toluenesulfonate In dichloromethane at 30℃; for 16h;89%

C45H67NO13

253128-41-5

(1S,3S,6S,9S,12S,14R,16R,18S,20R,21R,22S,26R,29S,31R,32S,33R,35R,36S)-20-[(2S)-3-Amino-2-hydroxypropyl]-21-methoxy-14-methyl-8,15-bis(methylene)-2,19,30,34,37,39,40,41-octaoxanonacyclo [24.9.2.13,32.13,33.16,9.112,16.018,22.029,36.031,35]hentetracontan-24-one

Conditions
ConditionsYield
Stage #1: C45H67NO13 With 2,6-dimethylpyridine; trimethylsilyl trifluoromethanesulfonate In dichloromethane at 0 - 20℃; for 2.5h;
Stage #2: With potassium carbonate In methanol at 20℃; for 2h;		88%
With 2,6-dimethylpyridine; trimethylsilyl trifluoromethanesulfonate In dichloromethane at 0 - 20℃; for 5.5h;1.6 mg
253128-40-4

(1S,3S,6S,9S,12S,14R,16R,18S,20R,21R,22S,26R,29S,31R,32S,33R,35R,36S)-20-[(2S)-3-azido-2-hydroxypropyl]-21-methoxy-14-methyl-8,15-bis(methylidene)-2,19,30,34,37,39,40,41-octaoxanonacyclo[24.9.2.13,32.13,33.16,9.112,16.018,22.029,36.031,35]hentetracontan-24-one

253128-41-5

(1S,3S,6S,9S,12S,14R,16R,18S,20R,21R,22S,26R,29S,31R,32S,33R,35R,36S)-20-[(2S)-3-Amino-2-hydroxypropyl]-21-methoxy-14-methyl-8,15-bis(methylene)-2,19,30,34,37,39,40,41-octaoxanonacyclo [24.9.2.13,32.13,33.16,9.112,16.018,22.029,36.031,35]hentetracontan-24-one

Conditions
ConditionsYield
With trimethylphosphane In tetrahydrofuran; water at 20℃; for 22h;87%
With water; trimethylphosphane In tetrahydrofuran at 20℃; for 22h; Staudinger Azide Reduction;87%
With triphenylphosphine In tetrahydrofuran; water at 21℃; for 24h; Inert atmosphere;
253128-19-7

C41H60O14S

253128-41-5

(1S,3S,6S,9S,12S,14R,16R,18S,20R,21R,22S,26R,29S,31R,32S,33R,35R,36S)-20-[(2S)-3-Amino-2-hydroxypropyl]-21-methoxy-14-methyl-8,15-bis(methylene)-2,19,30,34,37,39,40,41-octaoxanonacyclo [24.9.2.13,32.13,33.16,9.112,16.018,22.029,36.031,35]hentetracontan-24-one

Conditions
ConditionsYield
With ammonia In methanol at 20℃;
Multi-step reaction with 2 steps
1: tetrabutylammoniun azide / N,N-dimethyl-formamide / 3.5 h / 83 °C
2: trimethylphosphane; water / tetrahydrofuran / 22 h / 20 °C
View Scheme
253128-15-3

(1S,3S,6S,9S,12S,14R,16R,18S,20R,21R,22S,26R,29S,31R,32S,33R,35R,36S)-20-[(2S)-2,3-Dihydroxypropyl]-21-methoxy-14-methyl-8,15-bis(methylene)-2,19,30,34,37,39,40,41-octaoxanonacyclo[24.9.2.13,32.13,33.16,9.112,16.018,22.029,36.031,35]hentetracontan-24-one

253128-41-5

(1S,3S,6S,9S,12S,14R,16R,18S,20R,21R,22S,26R,29S,31R,32S,33R,35R,36S)-20-[(2S)-3-Amino-2-hydroxypropyl]-21-methoxy-14-methyl-8,15-bis(methylene)-2,19,30,34,37,39,40,41-octaoxanonacyclo [24.9.2.13,32.13,33.16,9.112,16.018,22.029,36.031,35]hentetracontan-24-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 90 percent / collidine / CH2Cl2 / 0 °C
2: NH3 / methanol / 20 °C
View Scheme
Multi-step reaction with 2 steps
1.1: 2,4,6-trimethyl-pyridine; pyridine / dichloromethane / -10 °C / Industrial scale
1.2: 10 - 30 °C / Industrial scale
2.1: ammonium hydroxide / dichloromethane; isopropyl alcohol / 10 - 30 °C / Industrial scale
View Scheme
Multi-step reaction with 3 steps
1: 2,4,6-trimethyl-pyridine / dichloromethane / 76.67 h / 0 - 4 °C
2: tetrabutylammoniun azide / N,N-dimethyl-formamide / 3.5 h / 83 °C
3: trimethylphosphane; water / tetrahydrofuran / 22 h / 20 °C
View Scheme
1190395-92-6

ER-809681

253128-41-5

(1S,3S,6S,9S,12S,14R,16R,18S,20R,21R,22S,26R,29S,31R,32S,33R,35R,36S)-20-[(2S)-3-Amino-2-hydroxypropyl]-21-methoxy-14-methyl-8,15-bis(methylene)-2,19,30,34,37,39,40,41-octaoxanonacyclo [24.9.2.13,32.13,33.16,9.112,16.018,22.029,36.031,35]hentetracontan-24-one

Conditions
ConditionsYield
With ammonium hydroxide In dichloromethane; isopropyl alcohol at 10 - 30℃; Industrial scale;
929121-23-3

(1R,2S,3S,4S,5S,6RS,11S,14S,17S,19R,21R,23S,25R,26R,27S,31R,34S)-25-[(2S)-2,3-dihydroxypropyl]-2,5-dihydroxy-26-methoxy-19-methyl-13,20-bis(methylene)-24,35,36,37,38,39-hexaoxaheptacyclo[29.3.1.13,6.14,34.111,14.117,21.023,27] nonatriacontane-8,29-dione

253128-41-5

(1S,3S,6S,9S,12S,14R,16R,18S,20R,21R,22S,26R,29S,31R,32S,33R,35R,36S)-20-[(2S)-3-Amino-2-hydroxypropyl]-21-methoxy-14-methyl-8,15-bis(methylene)-2,19,30,34,37,39,40,41-octaoxanonacyclo [24.9.2.13,32.13,33.16,9.112,16.018,22.029,36.031,35]hentetracontan-24-one

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: pyridinium p-toluenesulfonate / dichloromethane / 10 - 20 °C / Industrial scale
2.1: 2,4,6-trimethyl-pyridine; pyridine / dichloromethane / -10 °C / Industrial scale
2.2: 10 - 30 °C / Industrial scale
3.1: ammonium hydroxide / dichloromethane; isopropyl alcohol / 10 - 30 °C / Industrial scale
View Scheme

C63H111NO14Si3

253128-41-5

(1S,3S,6S,9S,12S,14R,16R,18S,20R,21R,22S,26R,29S,31R,32S,33R,35R,36S)-20-[(2S)-3-Amino-2-hydroxypropyl]-21-methoxy-14-methyl-8,15-bis(methylene)-2,19,30,34,37,39,40,41-octaoxanonacyclo [24.9.2.13,32.13,33.16,9.112,16.018,22.029,36.031,35]hentetracontan-24-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 20 h / 20 °C / Inert atmosphere
1.2: Dowex 50WX8-400 resin / 1 h
1.3: 1.5 h / 20 °C
2.1: 2,6-dimethylpyridine; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 2.5 h / 0 - 20 °C
2.2: 2 h / 20 °C
View Scheme

C45H69NO14

253128-41-5

(1S,3S,6S,9S,12S,14R,16R,18S,20R,21R,22S,26R,29S,31R,32S,33R,35R,36S)-20-[(2S)-3-Amino-2-hydroxypropyl]-21-methoxy-14-methyl-8,15-bis(methylene)-2,19,30,34,37,39,40,41-octaoxanonacyclo [24.9.2.13,32.13,33.16,9.112,16.018,22.029,36.031,35]hentetracontan-24-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: pyridinium p-toluenesulfonate / dichloromethane / 3 h / 20 °C
2: trimethylsilyl trifluoromethanesulfonate; 2,6-dimethylpyridine / dichloromethane / 5.5 h / 0 - 20 °C
View Scheme

C40H56O11

253128-41-5

(1S,3S,6S,9S,12S,14R,16R,18S,20R,21R,22S,26R,29S,31R,32S,33R,35R,36S)-20-[(2S)-3-Amino-2-hydroxypropyl]-21-methoxy-14-methyl-8,15-bis(methylene)-2,19,30,34,37,39,40,41-octaoxanonacyclo [24.9.2.13,32.13,33.16,9.112,16.018,22.029,36.031,35]hentetracontan-24-one

Conditions
ConditionsYield
With ammonium hydroxide In dichloromethane; water; isopropyl alcohol at 10 - 30℃; Solvent; Temperature;
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    253128-41-5 Eribulin

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  • Eribulin

  • Casno:

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    Eribulin

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    Suzhou Health Chemicals Co., Ltd. is A Fine Chemicals Company, specializing in research, development, manufacture and distribute raw materials for pharmaceutical, healthcare, bioch

  •  Suzhou Health Chemicals Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-512-58277800

    Address:No. 338, Jingang Avenue,

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    253128-41-5

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    Established in 2007, Win-Win chemical CO., Ltd is a privately held corporation headquartered in Wenzhou Longwan Industry Distric, dedicated to the global pharmaceutical companies a

  •  Win-Win chemical Co.Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:0086-577-64498589

    Address:No.49 YuShi West Road, Longwan District,325000

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    We are a Union of chemistry in China, consists of chemists，engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

    We are a Union of chemistry in China, consists of chemists，engineers, laboratories,factories in China. We organize surplus capacity of R&D and production in China for chemicals cus

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    China (Mainland)  |  Contact Details

    Business Type:Trading Company

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    Address:Liang Xi Qu

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    253128-41-5

    Eribulin

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    Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as:

    Chemfish co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L

  •  Hunan chemfish Pharmaceutical co.,Ltd

     China (Mainland)  |  Contact Details

    Business Type:Manufacturers

    Tel:0731-85567275

    Address:No.10048, xiangjiang centry bulding ,kaifu district ,changsha city ,Hunan

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    253128-41-5

    Eribulin

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    Wuhan Vanz Pharm Inc. is a manufacturer&trading company.

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     China (Mainland)  |  Contact Details

    Business Type:Manufacturers

    Tel:86-27-84492310

    Address:FANHU INDUSTRY PARK

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    253128-41-5

    253128-41-5 Eribulin

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    Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

    GIHI CHEMICALS CO.,LIMITED, its former company is a small manufacturer who is specialized in the production of ester products which are used in the daily chemicals ,cosmetic produc

  •  GIHI CHEMICALS CO.,LIMITED

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-86217390

    Address:No.567 Dengcai Street,Sandun,Westlake District,Hangzhou310030,Zhejiang,China.

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    253128-41-5

    Eribulin

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    Hangzhou Dingyan Chem Co., LTD. is located in the beautiful tourist city of hangzhou, is a comprehensive chemical enterprice which doing import and export business by its own comp

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     China (Mainland)  |  Contact Details

    Business Type:Manufacturers

    Tel:86-571-86465881,86-571-87157530,86-571-88025800

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    Eribulin

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    As a member of TAIHO Group,Hubei Taiho Chemical Co.,Ltd,is a professional new-type chemicals enterprise combined into research and development,production and sales.We adhere to the

  •  Hubei Taiho Chemical Co.,LTD

     China (Mainland)  |  Contact Details

    Business Type:Manufacturers

    Tel:+86-18120399543

    Address:No. 49 taifeng Road,Qianjiang City,Hubei,China

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    253128-41-5

    Eribulin

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    J&H CHEM is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other Value-added customer services, for diversified range products of chemicals

    J&H Chemical is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other

  •  Hangzhou J&H Chemical Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-87396432

    Address:No.200 Zhenhua Rd.Xihu Industrial Park, Hangzhou 310030, China

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  • Casno:

    253128-41-5

    Eribulin

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    best seller Application:API

    Xi'an Changyue Biotechnology Co., Ltd. was established in October 2003 and is located in Xi'an High-tech Industrial Development Park. It is a company specializing in the extraction

  •  Xian Changyue Biological Technology Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Manufacturers

    Tel:+86-029-62886900

    Address:Keji Road NO.70

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  • 253128-41-5 Eribulin

  • Casno:

    253128-41-5

    253128-41-5 Eribulin

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    253128-41-5 Eribulin Application:253128-41-5 Eribulin

    Hubei Xinrunde Chemical Co., Ltd. dedicated to the development, production and marketing of chemicals which is specialized in Organic compounds; Active Pharmaceutical Ingredient(s)

  •  Hubei Langyou International Trading Co., Ltd

    China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:+8618874586545

    Address:No.43, Xinandu Industrial Park, East and West Lake District, Wuhan, Hubei, China

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  • 253128-41-5 CAS No.253128-41-5

  • Casno:

    253128-41-5

    253128-41-5 CAS No.253128-41-5

    Min.Order: 0

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    Factory supply high purity low priceAppearance:solid or liquid Storage:sealed in cool and dry place Package:As customer's requested Application:Pharma Intermediate Transportation:by courier/air/sea Port:Any port in China

    Guangdong Juda Chemical Industrial Co.,Limited is a company specializing in APIs,pharmaceutical intermediates, electronic chemicals, plant extracts,fine chemicals and cosmetics raw

  •  Guangdong Juda Chemical Industrial Co.,Limited

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86 13510152023(whatsapp)

    Address:Guangzhou chemical city Tianhe District Guangzhou Guangdong China

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  • Eribulin

  • Casno:

    253128-41-5

    Eribulin

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    good quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:25kg,50kg,180kg,200kg,250kg,1000kg，customization Application:Pharma;Industry;Agricultural;chemical reaserch Tran

    Wuhan Circle Star Bio-medic Technology co.,Ltd is located in wuhan, the central city of China, the core of the Changjiang river economic belt and known as the "thoroughfare of nin

  •  Wuhan Circle Star Chem-medical Technology co.,Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-13437180835

    Address:Experimental Building 311-15, Nuclear Magnetic Spectrometer Industry Base, No. 128 Guanggu 7th Road, Donghu New Technology Development Zone, Wuhan (Wuhan Area, Free Trade Zone)

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  • Casno:

    253128-41-5

    Eribulin

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    best seller Application:API

    DB Biotech co., ltd is a global and professional supplier for plant extracts and functional ingredients, the company is based in XI’an city, which is famous city for the producttio

  •  DB BIOTECH CO., LTD

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86--1829 2989 553

    Address:No.99 Road, Xi'an, China

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  • Eribulin

  • Casno:

    253128-41-5

    Eribulin

    Min.Order: 0

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    Best quality with low price Storage:ln stock Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Shanghai

    Founded in 2005, Sartort, located in Hangzhou, is a leading company engaging in chemistry, pharmaceutical and advanced materials. At present, Sartort has such controlled subsidi

  •  Hangzhou Sartort Biopharma Co., Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-571-87039693

    Address:No. 57, Tech Park Road, Hangzhou, Zhejiang, China

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