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35205-54-0

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Basic Information
CAS No.: 35205-54-0
Name: 1-METHYL-2-PHENOXYETHYLAMINE
Article Data: 17
Molecular Structure:
Molecular Structure of 35205-54-0 (1-METHYL-2-PHENOXYETHYLAMINE)
Formula: C9H13NO
Molecular Weight: 151.208
Synonyms: 1-Phenoxypropan-2-amine;
Density: 1.004g/cm3
Melting Point: 147-148 °C
Boiling Point: 240.5°Cat760mmHg
Flash Point: 99.5°C
PSA: 35.25000
LogP: 2.11290
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Synthetic route
621-87-4

3-phenoxy-2-propanone

35205-54-0

1-methyl-2-phenoxyethylamine

Conditions
ConditionsYield
Stage #1: 3-phenoxy-2-propanone With ammonium formate In methanol at 80℃; for 0.166667h; Inert atmosphere;
Stage #2: With formic acid; C29H32ClIrNO; triethylamine In methanol at 80℃;		87%
With 4-methoxy-N-(1-(naphthalen-2-yl)ethylidene)aniline; ammonium formate In methanol at 80℃; for 12h; Inert atmosphere; chemoselective reaction;87%
Stage #1: 3-phenoxy-2-propanone With ammonium formate In methanol at 80℃; for 0.166667h; Inert atmosphere;
Stage #2: With formic acid; 4-methoxy-N-(1-(naphthalen-2-yl)ethylidene)aniline; triethylamine In methanol at 80℃; Inert atmosphere;		87%

1-Phenoxy-propan-2-one oxime

35205-54-0

1-methyl-2-phenoxyethylamine

Conditions
ConditionsYield
With hydrogen; nickel In isopropyl alcohol at 60℃; under 3102.9 Torr; 20-24 h;81%

2-(1-methyl-2-phenoxyethyl)-1H-isoindole-1,3(2H)-dione

35205-54-0

1-methyl-2-phenoxyethylamine

Conditions
ConditionsYield
With hydrazine hydrate; acetic acid In methanol for 4h; Reflux;56%
With hydrazine hydrate In ethanol
770-35-4

1-phenoxy-2-propanol

35205-54-0

1-methyl-2-phenoxyethylamine

Conditions
ConditionsYield
Stage #1: 1-phenoxy-2-propanol In dichloromethane cooling;
Stage #2: With dibenzyl azodicarboxylate In dichloromethane cooling;
Stage #3: With trifluoroacetic acid In dichloromethane Further stages.;		55%
30263-61-7

phenoxyacetone oxime

35205-54-0

1-methyl-2-phenoxyethylamine

Conditions
ConditionsYield
With nickel; benzene at 45℃; under 73550.8 Torr; Hydrogenation;
With diethyl ether; cyclohexane; nickel at 45℃; under 73550.8 Torr; Hydrogenation;
With lithium aluminium tetrahydride; diethyl ether
With lithium aluminium tetrahydride In diethyl ether for 12h; Heating;
With lithium aluminium tetrahydride In tetrahydrofuran for 3h; Reflux;
621-87-4

3-phenoxy-2-propanone

77287-34-4, 77287-35-5, 60100-09-6

formamide

35205-54-0

1-methyl-2-phenoxyethylamine

Conditions
ConditionsYield
Kochen des Reaktionsprodukts mit konz. wss. HCl;
108-95-2

phenol

35205-54-0

1-methyl-2-phenoxyethylamine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: sodium iodide; potassium carbonate / N,N-dimethyl-formamide
2: hydroxylamine hydrochloride; sodium hydroxide / 20 °C
3: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / Reflux
View Scheme
Multi-step reaction with 2 steps
1.1: potassium carbonate / acetone / 0.5 h / 20 °C
1.2: 3 h / Reflux
2.1: formamide / water / 4 h / 185 °C
View Scheme
35205-54-0

1-methyl-2-phenoxyethylamine

54750-12-8

(2R,4S,5R)-2-chloro-3,4-dimethyl-5-phenyl-1,3,2-oxazaphospholidin-2-one

((2R,4S,5R)-3,4-Dimethyl-5-phenyl-2-thioxo-2λ5-[1,3,2]oxazaphospholidin-2-yl)-(1-methyl-2-phenoxy-ethyl)-amine

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran RT, 24 h, 65 deg C, 24 h;100%
35205-54-0

1-methyl-2-phenoxyethylamine

108-24-7

acetic anhydride

68157-86-8

N-(1-methyl-2-phenoxyethyl)acetamide

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 0℃; Inert atmosphere;93%
35205-54-0

1-methyl-2-phenoxyethylamine

(2S)-4-methyl-2-isopropoxycarbonylaminopentanoic acid

(2S)-N-(1-methyl-2-phenoxyethyl)-4-methyl-2-(isopropoxycarbonylamino)pentanamide

Conditions
ConditionsYield
Stage #1: (2S)-4-methyl-2-isopropoxycarbonylaminopentanoic acid With isopropyl chloroformate; triethylamine In tetrahydrofuran at -3℃; for 1.5h;
Stage #2: 1-methyl-2-phenoxyethylamine In tetrahydrofuran at 20℃; for 5.5h;		83.2%
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