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Basic Information
CAS No.: 3695-77-0
Name: TRIPHENYLMETHYL MERCAPTAN
Article Data: 24
Molecular Structure:
Molecular Structure of 3695-77-0 (TRIPHENYLMETHYL MERCAPTAN)
Formula: C19H16 S
Molecular Weight: 276.402
Synonyms: Methanethiol,triphenyl- (7CI,8CI); Hydrotriphenylsulfur; NSC 22520; Triphenylmethanethiol;Triphenylmethyl mercaptan; Triphenylmethylthiol; Trityl mercaptan; Tritylthiol;a,a-Diphenylbenzenemethanethiol
EINECS: 223-020-3
Density: 1.119 g/cm3
Melting Point: 104-106 °C(lit.)
Boiling Point: 403.8 °C at 760 mmHg
Flash Point: 166.5 °C
Solubility: insoluble in water
Appearance: yellow-tan Powder
Hazard Symbols: HarmfulXn
Risk Codes: 20
Safety: Poison by intravenous route. When heated to decomposition it emits toxic fumes of SOx. See also SULFIDES.
PSA: 38.80000
LogP: 4.90830
Synthetic route
76-84-6

triphenylmethyl alcohol

3695-77-0

triphenylmethanethiol

Conditions
ConditionsYield
With Lawessons reagent In 1,2-dimethoxyethane for 15h; Mechanism; Ambient temperature; various alcohols, other solvents, other temperatures;100%
With Lawessons reagent In toluene for 0.2h; Quantum yield; Heating; DME, room temperature;100%
With Lawessons reagent In 1,2-dimethoxyethane for 15h; Ambient temperature;100%

N-methyl-3-(tritylthio)-maleimide

3695-77-0

triphenylmethanethiol

Conditions
ConditionsYield
With DL-dithiothreitol; triethylamine In tetrahydrofuran; water at 20℃; for 0.25h;96%
1727-15-7

trityl thioacetic acid

3695-77-0

triphenylmethanethiol

Conditions
ConditionsYield
With methanol; tetra-n-butylammonium cyanide In chloroform at 20℃; for 3h;92%

trans-2-chloro-1-(triphenylmethyldithio)cyclohexane

A

3695-77-0

triphenylmethanethiol

B

76-83-5

trityl chloride

C

C12H20Cl2S4

Conditions
ConditionsYield
In ethyl acetate for 13h; Heating;A 26%
B 23%
C 69%
80345-24-0

endo-2-chloro-exo-1-(triphenylmethyldithio)bicyclo<2.2.1>heptane

A

3695-77-0

triphenylmethanethiol

B

76-83-5

trityl chloride

C

di<(2-chloro)-1-norbornyl>tetrasulfide

Conditions
ConditionsYield
In ethyl acetate for 40h; Heating;A 21%
B 19%
C 68%
1277170-50-9

(1,1-dimethylethyl)dimethyl[[(triphenylmethyl)thio]methoxy]silane

3695-77-0

triphenylmethanethiol

Conditions
ConditionsYield
With tetrabutyl ammonium fluoride In tetrahydrofuran at -78℃; for 0.25h;68%
With tetrabutyl ammonium fluoride In tetrahydrofuran at -78 - -10℃; for 0.3h;68%

trans-2-chloro-1-(triphenylmethyltrithio)cyclopentane

A

3695-77-0

triphenylmethanethiol

B

76-83-5

trityl chloride

C

C10H16Cl2S4

Conditions
ConditionsYield
In ethyl acetate for 10h; Heating;A 27%
B 19%
C 67%

trans-2-chloro-1-(triphenylmethyldithio)cyclopentane

A

3695-77-0

triphenylmethanethiol

B

76-83-5

trityl chloride

C

C10H16Cl2S4

Conditions
ConditionsYield
In ethyl acetate for 8h; Heating;A 24%
B 20%
C 65%

trans-2-chloro-1-(triphenylmethyltrithio)cyclohexane

A

3695-77-0

triphenylmethanethiol

B

76-83-5

trityl chloride

C

C12H20Cl2S4

Conditions
ConditionsYield
In ethyl acetate for 15h; Heating;A 28%
B 21%
C 65%
513-81-5

2,3-dimethyl-buta-1,3-diene

A

3695-77-0

triphenylmethanethiol

B

18655-88-4

1,2-dithia-4,5-dimethyl-4-cyclohexene

C

139174-04-2

1,2,3,4-tetrathia-6,7-dimethyl-6-cyclooctene

D

C12H20Cl2S4

Conditions
ConditionsYield
With trans-2-chloro-1-(triphenylmethyltrithio)cyclohexane In ethyl acetate for 15h; Heating; Further byproducts given;A 29%
B 8%
C 63%
D 12%
With trans-2-chloro-1-(triphenylmethyldithio)cyclohexane In ethyl acetate for 10h; Heating; Further byproducts given;A 28%
B 10%
C 58%
D 16%
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  • TRIPHENYLMETHYL MERCAPTAN cas no. 3695-77-0 98%

  • Casno:

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    TRIPHENYLMETHYL MERCAPTAN cas no. 3695-77-0 98%

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  • Triphenylmethyl mercaptan

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    3695-77-0

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    3695-77-0

    Triphenylmethyl mercaptan

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  • TRIPHENYLMETHYL MERCAPTAN

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    3695-77-0

    TRIPHENYLMETHYL MERCAPTAN

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  • Acmec Triphenylmethyl Mercaptan 100g

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    3695-77-0

    Acmec Triphenylmethyl Mercaptan 100g

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    3695-77-0

    TRIPHENYLMETHYL MERCAPTAN

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  • Benzenemethanethiol, a,a-diphenyl-

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    3695-77-0

    Benzenemethanethiol, a,a-diphenyl-

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    3695-77-0

    TRIPHENYLMETHYL MERCAPTAN

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  • Triphenylmethyl mercaptan cas  3695-77-0

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    Triphenylmethyl mercaptan cas 3695-77-0

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  • TRIPHENYLMETHYL MERCAPTAN

  • Casno:

    3695-77-0

    TRIPHENYLMETHYL MERCAPTAN

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    Hangzhou Shanyi Biotechnology Co., Ltd. is headquartered in Hangzhou, China. It is a high-tech enterprise specializing in the research and development, production, development, and

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Chemistry

IUPAC Name:triphenylmethanethiol
Molecular Formula:C19H16S
Molecular Weight:276.395340 g/mol
Appearance:cream-pale yellow powder
Melting Point:104-106 °C(lit.)
Boiling Point:403.8 °C at 760 mmHg
Flash Point:166.5 °C
BRN:2113168
EINECS:223-020-3
Synonyms of TRIPHENYLMETHANETHIOL(3695-77-0):
TRIPHENYLMETHYL MERCAPTAN;TIMTEC-BB SBB007907;TRIPHENYLMETHYL MERCAPTAN;TRIPHENYLMETHANETHIOL;TRITYLTHIOL;TRITYL MERCAPTAN;alpha,alpha-diphenyl-benzenemethanethio;alpha,alpha-diphenylbenzenemethanethiol;Benzenemethanethiol, alpha,alpha-diphenyl-

Toxicity Data With Reference

1.   

ivn-mus LD50:180 mg/kg

   CSLNX*    U.S. Army Armament Research & Development Command, Chemical Systems Laboratory, NIOSH Exchange Chemicals. (Aberdeen Proving Ground, MD 21010) NX#04016 .

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Safety Information of TRIPHENYLMETHANETHIOL(3695-77-0):
Hazard Codes:Xn
Risk Statements:20
20:Harmful by inhalation
Safety Statements:23
23:Do not breathe gas/fumes/vapor/spray (appropriate wording to be specified by the manufacturer)
WGK Germany:3
RTECS:PB5335000
F:10-13
Poison by intravenous route. When heated to decomposition it emits toxic fumes of SOx. See also SULFIDES.

Specification

First Aid Measures of TRIPHENYLMETHANETHIOL(3695-77-0):
Eyes:Flush eyes with plenty of water for at least 15 minutes, occasionally lifting the upper and lower eyelids. Get medical aid immediately.
Skin:Get medical aid. Flush skin with plenty of water for at least 15 minutes while removing contaminated clothing and shoes. Remove contaminated clothing and shoes.
Ingestion:If victim is conscious and alert, give 2-4 cupfuls of milk or water. Get medical aid immediately.
Inhalation:Get medical aid immediately. Remove from exposure and move to fresh air immediately. If not breathing, give artificial respiration. If breathing is difficult, give oxygen.

Storage of TRIPHENYLMETHANETHIOL(3695-77-0):
Store in a cool, dry place. Keep container closed when not in use.