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CAS No.: | 39484-81-6 |
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Name: | Diazenecarbothioamide, N,N-diethyl-2-phenyl- |
Article Data: | 4 |
Molecular Structure: | |
Formula: | C11H15N3S |
Molecular Weight: | 221.326 |
Synonyms: | Diazenecarbothioamide,N,N-diethyl-2-phenyl;N,N-Diethylphenylazothioformamid;N,N-diethyl-(2-phenyldiazenyl)thioformamide; |
PSA: | 60.05000 |
LogP: | 3.39700 |
carbon disulfide
diethylamine
phenylhydrazine
N,N-diethyl-(2-phenyldiazenyl)thioformamide
Conditions | Yield |
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Stage #1: carbon disulfide; phenylhydrazine In ethanol for 0.5h; Inert atmosphere; Stage #2: With potassium hydroxide In ethanol for 0.5h; Inert atmosphere; Stage #3: diethylamine Further stages; | 68% |
4,4-diethyl-1-phenylthiosemicarbazide
N,N-diethyl-(2-phenyldiazenyl)thioformamide
Conditions | Yield |
---|---|
With oxygen; diethylamine at 20℃; for 24h; | 53.23 g |
phenylhydrazine
N,N-diethyl-(2-phenyldiazenyl)thioformamide
Conditions | Yield |
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Multi-step reaction with 3 steps 1.1: ethanol / 0.25 h 1.2: KOH / ethanol / 0.5 h 2.1: 72 h / Heating 3.1: 53.23 g / oxygen; diethylamine / 24 h / 20 °C View Scheme |
methyl 2-phenylhydrazinecarbodithioate
N,N-diethyl-(2-phenyldiazenyl)thioformamide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 72 h / Heating 2: 53.23 g / oxygen; diethylamine / 24 h / 20 °C View Scheme |