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Basic Information
| CAS No.: | 46032-98-8 |
|---|---|
| Name: | (1R,2R)-(-)-2-Amino-1-phenyl-1,3-propanediol |
| Article Data: | 45 |
| Molecular Structure: | |
|
|
|
| Formula: | C9H13 N O2 |
| Molecular Weight: | 167.208 |
| Synonyms: | 1,3-Propanediol,2-amino-1-phenyl-, [R-(R*,R*)]-; (1R,2R)-(-)-2-Amino-1-phenyl-1,3-propanediol;(1R,2R)-2-Amino-1-phenylpropane-1,3-diol;D-threo-1-Phenyl-2-amino-1,3-propanediol;D-threo-3-Phenyl-2-amino-1,3-propanediol |
| EINECS: | 256-250-8 |
| Density: | 1.206 g/cm3 |
| Melting Point: | 112 - 115 C |
| Boiling Point: | 360.6 °C at 760 mmHg |
| Flash Point: | 171.9 °C |
| Appearance: | light yellow powder |
| Hazard Symbols: |
|
| Risk Codes: | R36/37/38 |
| Safety: | 26-36-37/39 |
| Transport Information: | UN 3259 |
| PSA: | 66.48000 |
| LogP: | 0.73990 |
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Synthetic route
- 912296-87-8
syn-(2R,3R)-[2-azido-3-hydroxy-3-phenyl-1-propanol]
- 46032-98-8
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions
| Conditions | Yield |
|---|---|
| With hydrogen; palladium on activated charcoal In methanol at 20℃; under 760 Torr; for 12h; | 99% |
- 849357-84-2
(2S,3R)-2-Azido-3-nitrosooxy-3-phenyl-propionic acid methyl ester
- 46032-98-8
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions
| Conditions | Yield |
|---|---|
| With hydrogen; palladium on activated charcoal In methanol at 20℃; under 760 Torr; for 12h; | 97% |
- 3306-06-7, 5285-86-9, 28143-91-1, 36391-67-0, 36391-68-1, 46032-98-8, 55057-81-3, 105452-39-9, 119364-52-2
(+/-)-threo-2-amino-1-phenyl-1,3-propanediol
- 46032-98-8
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions
| Conditions | Yield |
|---|---|
| With L-Tartaric acid | |
| With L-(-)-O,O'-dibenzoyltartaric acid | |
| With (1S)-(+)-3-bromocamphor-10-sulfonic acid | |
| With D-Glutamic acid |
- 114530-99-3
(2S,3R)-2-amino-3-hydroxy-3-phenyl-propionic acid cyclohexyl ester
- 46032-98-8
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions
| Conditions | Yield |
|---|---|
| With lithium aluminium tetrahydride; diethyl ether |
- 91247-54-0
1-Phenyl-2-acetamido-1,3-propandiol
A
- 28143-91-1
(1S,2S)-2-amino-1-phenyl-1,3-diol
B
- 46032-98-8
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
C
- 105452-39-9
(1R,2S)-(+)-2-amino-1-phenyl-1,3-propanediol
D
- 119364-52-2
(1S,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions
| Conditions | Yield |
|---|---|
| hydrolysis; |
...Expand
- 46032-98-8
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions
| Conditions | Yield |
|---|---|
| With lithium aluminium tetrahydride In tetrahydrofuran for 4h; Heating; |
- 285567-86-4
(1R,2R)-2-amino-(N-benzyloxycarbonyl)-1-phenylpropane-1,3-diol
- 46032-98-8
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions
| Conditions | Yield |
|---|---|
| With hydrogen |
Conditions
| Conditions | Yield |
|---|---|
| With (1S)-(+)-3-bromocamphor-10-sulfonic acid; ethyl acetate |
- 46032-98-8
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions
| Conditions | Yield |
|---|---|
| With (1S)-(+)-3-bromocamphor-10-sulfonic acid; ethyl acetate |
- 46032-98-8
(1R,2R)-2-amino-1-phenylpropane-1,3-diol
Conditions
| Conditions | Yield |
|---|---|
| With 1,4-dioxane; sodium tetrahydroborate und Erwaermen des Reaktionsprodukts mit wss.HCl; |
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(1R,2R)-(-)-2-Amino-1-phenyl-1,3-propanediol
Chemistry
IUPAC Name: (1R,2R)-2-amino-1-phenylpropane-1,3-diol
The MF of (1R,2R)-(-)-2-Amino-1-phenyl-1,3-propanediol(46032-98-8): C9H13NO2
The MW of (1R,2R)-(-)-2-Amino-1-phenyl-1,3-propanediol(46032-98-8): 167.21
EINECS: 256-250-8
mp: 112-118 °C(lit.)
alpha: -39 °(c=1, 1N HCl)
refractive index: -26.5 ° (C=1, MeOH)
Molar Refractivity: 47 cm3
Molar Volume: 138.5 cm3
Polarizability: 18.63 10-24 cm3
Surface Tension: 57.8 dyne/cm
Density: 1.206 g/cm3
Flash Point: 171.9 °C
Enthalpy of Vaporization: 63.98 kJ/mol
Boiling Point: 360.6 °C at 760 mmHg
Vapour Pressure: 7.87E-06 mmHg at 25°C
Categories: Amino Alcohols (Chiral);Asymmetric Synthesis;Chiral Building Blocks;Synthetic Organic Chemistry;Amino Alcohols;Chiral Building Blocks;Organic Building Blocks
Synonyms: (1R,2R)-(-)-2-AMINO-1-PHENYL-1,3-PROPANEDIOL;(1R,2R)-2-AMINO-1-PHENYLPROPANE-1,3-DIOL;(2R,3R)-3-PHENYLSERINOL;(2R,3S)-PHENYLSERINOL;[R(R*,R*)]-2-amino-1-phenylpropane-1,3-diol;(1R,2S)-3-Phenylserinol;1,3-Propanediol, 2-amino-1-phenyl-, [R-(R*,R*)]-;(1R,2R)-1-Phenyl-2-amino-1,3-propanediol
The Structure of (1R,2R)-(-)-2-Amino-1-phenyl-1,3-propanediol(46032-98-8):
The MF of (1R,2R)-(-)-2-Amino-1-phenyl-1,3-propanediol(46032-98-8): C9H13NO2
The MW of (1R,2R)-(-)-2-Amino-1-phenyl-1,3-propanediol(46032-98-8): 167.21
EINECS: 256-250-8
mp: 112-118 °C(lit.)
alpha: -39 °(c=1, 1N HCl)
refractive index: -26.5 ° (C=1, MeOH)
Molar Refractivity: 47 cm3
Molar Volume: 138.5 cm3
Polarizability: 18.63 10-24 cm3
Surface Tension: 57.8 dyne/cm
Density: 1.206 g/cm3
Flash Point: 171.9 °C
Enthalpy of Vaporization: 63.98 kJ/mol
Boiling Point: 360.6 °C at 760 mmHg
Vapour Pressure: 7.87E-06 mmHg at 25°C
Categories: Amino Alcohols (Chiral);Asymmetric Synthesis;Chiral Building Blocks;Synthetic Organic Chemistry;Amino Alcohols;Chiral Building Blocks;Organic Building Blocks
Synonyms: (1R,2R)-(-)-2-AMINO-1-PHENYL-1,3-PROPANEDIOL;(1R,2R)-2-AMINO-1-PHENYLPROPANE-1,3-DIOL;(2R,3R)-3-PHENYLSERINOL;(2R,3S)-PHENYLSERINOL;[R(R*,R*)]-2-amino-1-phenylpropane-1,3-diol;(1R,2S)-3-Phenylserinol;1,3-Propanediol, 2-amino-1-phenyl-, [R-(R*,R*)]-;(1R,2R)-1-Phenyl-2-amino-1,3-propanediol
The Structure of (1R,2R)-(-)-2-Amino-1-phenyl-1,3-propanediol(46032-98-8):
Safety Profile
Hazard Codes: 
Xi
Risk Statements: 36/37/38
36/37/38: Irritating to eyes, respiratory system and skin
Safety Statements: 26-36-37/39
26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
36: Wear suitable protective clothing
37/39: Wear suitable gloves and eye/face protection
RIDADR: UN 3259 8/PG 3
WGK Germany: 3
Xi Risk Statements: 36/37/38
36/37/38: Irritating to eyes, respiratory system and skin
Safety Statements: 26-36-37/39
26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
36: Wear suitable protective clothing
37/39: Wear suitable gloves and eye/face protection
RIDADR: UN 3259 8/PG 3
WGK Germany: 3
Specification
1. First Aid Measures
Ingestion:
Get medical aid. Wash mouth out with water.
Inhalation:
Remove from exposure to fresh air immediately. If not breathing, give artificial respiration. If breathing is difficult, give oxygen. Get medical aid.
Skin:
Get medical aid. Flush skin with plenty of soap and water for at least 15 minutes while removing contaminated clothing and shoes.
Eyes:
Flush eyes with plenty of water for at least 15 minutes, occasionally lifting the upper and lower eyelids. Get medical aid.
2. Handling and Storage
Storage:
Store in a cool, dry place. Store in a tightly closed container.
Handling:
Avoid breathing dust, vapor, mist, or gas. Avoid contact with skin and eyes.
Ingestion:
Get medical aid. Wash mouth out with water.
Inhalation:
Remove from exposure to fresh air immediately. If not breathing, give artificial respiration. If breathing is difficult, give oxygen. Get medical aid.
Skin:
Get medical aid. Flush skin with plenty of soap and water for at least 15 minutes while removing contaminated clothing and shoes.
Eyes:
Flush eyes with plenty of water for at least 15 minutes, occasionally lifting the upper and lower eyelids. Get medical aid.
2. Handling and Storage
Storage:
Store in a cool, dry place. Store in a tightly closed container.
Handling:
Avoid breathing dust, vapor, mist, or gas. Avoid contact with skin and eyes.