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CAS No.: | 55-81-2 |
---|---|
Name: | 4-Methoxyphenethylamine |
Article Data: | 85 |
Molecular Structure: | |
Formula: | C9H13NO |
Molecular Weight: | 151.208 |
Synonyms: | Phenethylamine,p-methoxy- (6CI,8CI);2-(4-Methoxyphenyl)ethanamine;2-(4-Methoxyphenyl)ethylamine;2-(p-Methoxyphenyl)ethylamine;4-Methoxy-b-phenethylamine;4-Methoxy-b-phenylethylamine;4-Methoxybenzeneethanamine;4-Methoxyphenethylamine;4-Methoxyphenylethylamine;Homoanisylamine;NSC 43687;O-Methyltyramine;Tyramine, O-methyl-;p-Methoxyphenethylamine; |
EINECS: | 200-245-5 |
Density: | 1.008 g/cm3 |
Melting Point: | 249-251°C |
Boiling Point: | 255.2 °C at 760 mmHg |
Flash Point: | 105.3 °C |
Appearance: | clear colorless to slightly yellow liquid |
Hazard Symbols: | C |
Risk Codes: | 34 |
Safety: | 26-36/37/39-45 |
Transport Information: | UN 2735 |
PSA: | 35.25000 |
LogP: | 1.89670 |
benzyl 4-methoxyphenethylcarbamate
4-Methoxyphenethylamine
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; hydrogen In methanol at 20℃; for 1h; | 100% |
Conditions | Yield |
---|---|
With aluminum (III) chloride; lithium aluminium tetrahydride In diethyl ether at 0 - 20℃; | 96% |
With lithium borohydride; diisopropopylaminoborane In tetrahydrofuran for 18h; Reflux; | 94% |
With [Ru(H)(BH4)(CO)(PPh3)(3-(di-tert-butylphosphino)-N-((1-methyl-1H-imidazol-2 yl)methyl)propylamine)]; hydrogen In isopropyl alcohol at 70℃; for 3h; Inert atmosphere; Autoclave; | 94% |
lysichitalexin
4-Methoxyphenethylamine
Conditions | Yield |
---|---|
With samarium diiodide; water; isopropylamine In tetrahydrofuran | 96% |
4-Methoxyphenethylamine
Conditions | Yield |
---|---|
With potassium carbonate; thiophenol In acetonitrile at 50℃; | 95% |
C12H14Cl3NO3
4-Methoxyphenethylamine
Conditions | Yield |
---|---|
Stage #1: C12H14Cl3NO3 With chloro-trimethyl-silane; mischmetal In tetrahydrofuran for 2h; Inert atmosphere; Reflux; Stage #2: With water In tetrahydrofuran for 0.0833333h; Alkaline conditions; | 87% |
Conditions | Yield |
---|---|
With hydrogenchloride; hydrogen; acetic acid; palladium on activated charcoal for 1h; | 71% |
With hydrogen; carbon palladium at 85℃; under 37503 Torr; | 70% |
(catalytic hydrogenation); |
2-4-methoxyphenylethylcarbamic acid methyl ester
A
7-methoxy-3,4-dihydro-2H-isoquinolin-1-one
B
4-Methoxyphenethylamine
Conditions | Yield |
---|---|
With PPA at 145℃; for 0.166667h; | A 59% B 30% |
3-(4-methoxy-phenyl)propionamide
4-Methoxyphenethylamine
Conditions | Yield |
---|---|
With sodium hydroxide; bromine In water at 70 - 80℃; for 0.25h; | 53% |
With sodium hypobromide | |
With alkaline sodium hypochlorite |
4-methyl-N-[2-(4-methoxyphenyl)ethyl]benzenesulfonamide
4-Methoxyphenethylamine
Conditions | Yield |
---|---|
With titanium tetrachloride In tetrahydrofuran for 2.5h; Heating; | 40% |
(E)-1-methoxy-4-(2-nitrovinyl)benzene
4-Methoxyphenethylamine
Conditions | Yield |
---|---|
With samarium diiodide; water; isopropylamine In tetrahydrofuran | 36% |
With sulfuric acid; palladium; acetic acid Hydrogenation; | |
bei der elektrochemischen Reduktion; | |
With lithium aluminium tetrahydride |
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1. | ipr-mus LD50:100 mg/kg | NTIS** National Technical Information Service. (Springfield, VA 22161) (Formerly U.S. Clearinghouse for Scientific and Technical Information) No. AD277-689 . |
Poison by intraperitoneal route. When heated to decomposition it emits toxic fumes of NOx.
Hazard Codes:C,T
C:Corrosive
T:Toxic
Risk Statements
R34:Causes burns.
Safety Statements
S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection .
S45:In case of accident or if you feel unwell, seek medical advice immediately (show label where possible) .
S27:Take off immediately all contaminated clothing .
RIDADR:
UN 2735 8/PG 3
WGK Germany:3
RTECS:SH7875000
F:10-23
Hazard Note:Toxic/Corrosive
HS Code:29222900