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| CAS No.: | 5523-19-3 |
|---|---|
| Name: | BORON TRICHLORIDE-METHYL SULFIDE COMPLEX |
| Article Data: | 2 |
| Molecular Structure: | |
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|
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| Formula: | C2H6BCl3S |
| Molecular Weight: | 179.306 |
| Synonyms: | TRICHLOROBORANE-METHYL SULFIDE;DIMETHYL SULFIDE-TRICHLOROBORANE;BORON TRICHLORIDE-METHYL SULFIDE COMPLEX;Boron trichloride-methyl sulfide complex solution;BORON TRICHLORIDE-METHYL SULFIDE COMPLEX , 2.0M SOLUTION IN DICHLOROMETHANE;Boron, trichlorothiobismethane-, (T-4)-;Borane-trichloride-methyl sulfide complex;Dimethyl sulfide-trichloroborane, Trichloroborane-methyl sulfide |
| Density: | 1.344 g/mL at 25 °C |
| Melting Point: | 88-90 °C(lit.) |
| Hazard Symbols: | C |
| Risk Codes: | 34-40-20/21/22-67-37 |
| Safety: | 26-27-28-36/37/39-45 |
| PSA: | 19.21000 |
| LogP: | 2.66690 |
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- 894852-01-87-BROMO-2,2-DIMETHYL-2H-PYRIDO[3,2-B][1,4]OXAZIN-3(4H)-ONE
- 74-85-1
ethene
- 63348-81-2
monochloroborane dimethyl sulfide complex
- 10294-34-5
boron trichloride
A
- 87115-49-9
C2H5(H)BCl
B
- 5314-83-0
diethylchloroborane
C
- 5523-19-3
boron trichloride - methyl sulfide complex
| Conditions | Yield |
|---|---|
| In pentane inert. atmosphere; bubbling C2H4 into H2BClSMe2 soln. (4.5 h), cooling in liquid N2, BCl3 addn.; fractional distn. (42°C, 200 Torr); | A n/a B 90% C n/a |
- 2102-03-6
boron trichloride-diethyl ether
- 75067-06-0
thexylchloroborane*methyl sulfide
A
- 79200-91-2
(CH3)2CHC(CH3)2BCl2(S(CH3)2)
B
- 79200-86-5
(CH3)2CHC(CH3)2BHCl(O(C2H5)2)
C
- 5523-19-3
boron trichloride - methyl sulfide complex
D
- 37099-64-2
[(1,1,2-trimethylpropyl)borane]2
| Conditions | Yield |
|---|---|
| In diethyl ether 0 °C, 1 h; |
| Conditions | Yield |
|---|---|
| In hexane Inert atmosphere; | 98% |
- 4375-83-1
tris(dimethylamino)borane
- 5523-19-3
boron trichloride - methyl sulfide complex
- 6562-41-0
chloro-bis(dimethylamino)borane
| Conditions | Yield |
|---|---|
| at 20 - 25℃; for 17 - 19h; Neat (no solvent); Heating / reflux; | 93.3% |
- 867-97-0
tris(diethylamino)borane
- 5523-19-3
boron trichloride - methyl sulfide complex
- 868-25-7
bis(diethylamino)boron chloride
| Conditions | Yield |
|---|---|
| In neat (no solvent) stirring for 2 h at room temp.; distn.; | 85% |
- 5523-19-3
boron trichloride - methyl sulfide complex
- 1253239-76-7
tris[2-(1,3,5-dithiazinan-5-yl)ethanyl] boric ester
- 1253240-06-0
tris[2-(5-trichloroborane-1,3,5-dithiazinan-5-yl)ethanyl] boric ester trichloroborane adduct
| Conditions | Yield |
|---|---|
| In toluene at -5 - 20℃; | 80% |
- 5523-19-3
boron trichloride - methyl sulfide complex
- 109-89-7
diethylamine
- 867-97-0
tris(diethylamino)borane
| Conditions | Yield |
|---|---|
| In cyclohexane (under N2), addn. of BCl3(Me2S) to a soln. of the amine in cyclohexane at 40°C over 1 h, refluxing for 1.5 h; the pptd. hydrochloride was filtered off after cooling and washed with cyclohexane; concn. and distn. of the filtrate;; | 78% |
- 1630-79-1
tetrakis(dimethylamido)diborane
- 5523-19-3
boron trichloride - methyl sulfide complex
A
- 1113-31-1
dichlorodimethylaminoborane
| Conditions | Yield |
|---|---|
| In benzene at 20 - 80℃; Inert atmosphere; | A n/a B n/a C 67% |
| Conditions | Yield |
|---|---|
| In dichloromethane for 2h; Inert atmosphere; | 65% |
- 23936-60-9
1,2-bis(dimethylphosphanyl)ethane
- 5523-19-3
boron trichloride - methyl sulfide complex
| Conditions | Yield |
|---|---|
| In dichloromethane for 1h; Inert atmosphere; | 56% |
- Total:15 Page 1 of 1 1
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