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| CAS No.: | 628-90-0 |
|---|---|
| Name: | 2,4,6-Trioxaheptane |
| Article Data: | 34 |
| Molecular Structure: | |
|
|
|
| Formula: | C4H10O3 |
| Molecular Weight: | 106.122 |
| Synonyms: | 17beta-methoxymethyl ether;Bis-methoxymethyl-aether;bis-methoxymethyl ether;METHOXY-(METHOXYMETHOXY)METHANE;methoxy-methyl ether; |
| Density: | 0.933g/cm3 |
| Melting Point: | -65 °C |
| Boiling Point: | 64.1°C at 760 mmHg |
| Flash Point: | 7.3°C |
| PSA: | 27.69000 |
| LogP: | 0.21080 |
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| Conditions | Yield |
|---|---|
| With sulfonic acid resin at 80 - 95℃; Temperature; Reagent/catalyst; | 95.5% |
| With ZrO2#dotLa2O3 at 80℃; for 4h; | 6.1% |
| With C16H36NO3S(1+)*CH3O4S(1-) at 125 - 130℃; under 26252.6 - 30003 Torr; Reagent/catalyst; Inert atmosphere; |
| Conditions | Yield |
|---|---|
| In ethyl acetate; N,N-dimethyl-formamide; mineral oil | 90% |
- 50-00-0
formaldehyd
- 109-87-5
Dimethoxymethane
A
- 13353-03-2
bis-methoxymethoxy-methane
B
- 628-90-0
bis(methoxymethyl)ether
| Conditions | Yield |
|---|---|
| With sulfuric acid at 109.99℃; under 7500.75 Torr; | A n/a B 26% |
- 67-56-1
methanol
- 50-00-0
formaldehyd
A
- 13353-03-2
bis-methoxymethoxy-methane
B
- 628-90-0
bis(methoxymethyl)ether
C
- 13352-75-5
POMM4
| Conditions | Yield |
|---|---|
| With ZrO2#dotLa2O3 at 130℃; under 6000.6 Torr; for 4h; Pressure; Reagent/catalyst; | A 23% B 23.3% C 14.9% |
- 50-00-0
formaldehyd
- 109-87-5
Dimethoxymethane
A
- 13353-03-2
bis-methoxymethoxy-methane
B
- 628-90-0
bis(methoxymethyl)ether
C
- 13352-75-5
POMM4
| Conditions | Yield |
|---|---|
| With La2O3 doped titania at 130℃; under 4500.45 Torr; for 4h; Reagent/catalyst; Pressure; Autoclave; | A 22.4% B 17.5% C 8.4% |
| With macroporous strong acidic styrene type cation exchange resin catalyst at 100℃; under 15001.5 Torr; for 10h; Temperature; Time; Overall yield = 51.66 %; | |
| With Cl -/TiO2-La2O3/SBA-15 (Si/Al=38) at 130℃; under 4500.45 Torr; for 4h; Reagent/catalyst; Temperature; Pressure; |
| Conditions | Yield |
|---|---|
| With naphthalene; lithium In tetrahydrofuran; water |
- 110-88-3
1,3,5-Trioxan
- 534-15-6
1,1-dimethoxyethane
C
- 13353-03-2
bis-methoxymethoxy-methane
D
- 628-90-0
bis(methoxymethyl)ether
E
- 13352-75-5
POMM4
F
- 13352-78-8
CH3-(OCH2)8-OCH3
G
- 54261-86-8
Methoxymethoxymethoxymethoxymethoxy-methoxymethoxymethoxymethoxymethoxymethoxy-methane
H
- 13352-76-6
POMM5
I
- 13353-04-3
CH3-(OCH2)7-OCH3
J
- 13352-77-7
CH3-(OCH2)6-OCH3
| Conditions | Yield |
|---|---|
| Amberlite IR 120 at 100℃; for 24h; Product distribution / selectivity; | |
| trifluorormethanesulfonic acid at 100℃; for 40h; Product distribution / selectivity; | |
| sulfuric acid In water at 100℃; for 12h; Product distribution / selectivity; |
- 110-88-3
1,3,5-Trioxan
- 534-15-6
1,1-dimethoxyethane
A
- 13353-03-2
bis-methoxymethoxy-methane
B
- 628-90-0
bis(methoxymethyl)ether
C
- 13352-75-5
POMM4
| Conditions | Yield |
|---|---|
| sulfuric acid In water at 100℃; for 16h; Product distribution / selectivity; |
- 50-00-0
formaldehyd
- 534-15-6
1,1-dimethoxyethane
C
- 13353-03-2
bis-methoxymethoxy-methane
D
- 628-90-0
bis(methoxymethyl)ether
E
- 13352-75-5
POMM4
F
- 13352-78-8
CH3-(OCH2)8-OCH3
G
- 54261-86-8
Methoxymethoxymethoxymethoxymethoxy-methoxymethoxymethoxymethoxymethoxymethoxy-methane
H
- 13352-76-6
POMM5
I
- 13353-04-3
CH3-(OCH2)7-OCH3
J
- 13352-77-7
CH3-(OCH2)6-OCH3
| Conditions | Yield |
|---|---|
| Amberlite IR 120 at 100℃; for 8h; Product distribution / selectivity; |
- 50-00-0
formaldehyd
- 109-87-5
Dimethoxymethane
A
- 110-88-3
1,3,5-Trioxan
D
- 13353-03-2
bis-methoxymethoxy-methane
E
- 628-90-0
bis(methoxymethyl)ether
F
- 13352-75-5
POMM4
G
- 13352-78-8
CH3-(OCH2)8-OCH3
H
- 54261-86-8
Methoxymethoxymethoxymethoxymethoxy-methoxymethoxymethoxymethoxymethoxymethoxy-methane
I
- 13353-04-3
CH3-(OCH2)7-OCH3
L
- 13352-77-7
CH3-(OCH2)6-OCH3
| Conditions | Yield |
|---|---|
| With sulfuric acid at 55 - 115℃; Inert atmosphere; |
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- Total:29 Page 1 of 1 1
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