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Basic Information
CAS No.: 6323-18-8
Name: 2-chloropropiophenone
Article Data: 13
Molecular Structure:
Molecular Structure of 6323-18-8 (2-chloropropiophenone)
Formula: C9H9 Cl O
Molecular Weight: 168.623
Synonyms: Propiophenone,2'-chloro- (6CI,7CI); 2'-Chloropropiophenone; NSC 32597; o-Chloropropiophenone
Density: 1.128±0.06 g/cm3(Predicted)
Boiling Point: 115-116℃ (15 Torr)
PSA: 17.07000
LogP: 2.93270
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Conditions
ConditionsYield
With pyridinium chlorochromate In dichloromethane at 20℃; for 2h;99%
With chromium(VI) oxide; sulfuric acid In acetone for 2h;
With chromium(VI) oxide; sulfuric acid In water; acetone at 10℃; Jones oxidation;
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ethylmagnesium bromide

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Conditions
ConditionsYield
Stage #1: 2-Chlorobenzonitrile; ethylmagnesium bromide
Stage #2: With water Further stages.;		89%
Stage #1: 2-Chlorobenzonitrile; ethylmagnesium bromide
Stage #2: With sulfuric acid		79%
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2'-Aminopropiophenon

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Conditions
ConditionsYield
With hydrogenchloride; copper(l) chloride at 70℃;
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ethylmagnesium iodide

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Conditions
ConditionsYield
(i), (ii) aq. H2SO4; Multistep reaction;
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o-chlorobenzoyl chloride

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Conditions
ConditionsYield
(i) Mg, I2, EtOH, CCl4, benzene, (ii) /BRN= 386435/; Multistep reaction;
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2-chloro-benzaldehyde

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2-chloropropiophenone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: tetrahydrofuran / 0.33 h / -78 - 20 °C
1.2: 65 percent / 4 h / 20 °C
2.1: 99 percent / PCC / CH2Cl2 / 2 h / 20 °C
View Scheme
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2-chloro-benzaldehyde

(+-)-piperoin

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Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: diethyl ether
2: CrO3; H2SO4 / acetone; H2O / 10 °C
View Scheme
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2-Chlorobenzonitrile

A

6323-18-8

2-chloropropiophenone

B

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2-bromo-2'-chloropropiophenone

sesquiethylaluminum chloride dimer

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o-chlorobenzoyl chloride

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Conditions
ConditionsYield
With aluminium trichloride at 40℃;
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methanol

6323-18-8

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1-(2-chlorophenyl)-2-methyl-propan-1-one

Conditions
ConditionsYield
With C34H27IrN2P(1+)*C32H12BF24(1-); caesium carbonate at 65℃; for 24h; Inert atmosphere;89%
Raw Materials
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    Shanghai AngewChemCo., Ltd. is an innovative enterprise on fine chemicals and pharmaceuticals. Based on Shanghai R&D center and Hunan chemical manufacturing plant, we offer chemical research, process development, and large-scale production. Complete

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     China (Mainland)  |  Contact Details

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