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| CAS No.: | 65193-87-5 |
|---|---|
| Name: | 3-Bromopropionaldehydedimethylacetal |
| Article Data: | 16 |
| Molecular Structure: | |
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|
|
| Formula: | C7H9 N O3 |
| Molecular Weight: | 155.153 |
| Synonyms: | 2-Cyanoethylacetoacetate; b-Cyanoethylacetoacetate |
| Density: | 1.124g/cm3 |
| Boiling Point: | 288.196°C at 760 mmHg |
| Flash Point: | 124.214°C |
| PSA: | 80.99000 |
| LogP: | -0.61062 |
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- 914458-26-7[5-(2-fluorophenyl)-1-pentyl-1H-pyrrol-3-yl]-1-naphthalenyl-Methanone
- 894852-01-87-BROMO-2,2-DIMETHYL-2H-PYRIDO[3,2-B][1,4]OXAZIN-3(4H)-ONE
- 5394-63-8
2,2,6-trimethyl-4H-1,3-dioxin-4-one
- 109-78-4
3-Hydroxypropionitrile
- 65193-87-5
2-cyanoethylacetoacetate
| Conditions | Yield |
|---|---|
| In o-xylene at 141℃; for 2h; | 98.3% |
| In 5,5-dimethyl-1,3-cyclohexadiene at 140 - 145℃; for 1h; | 90% |
| In xylene at 140 - 145℃; for 1h; | 81.6% |
- 105-45-3
acetoacetic acid methyl ester
- 109-78-4
3-Hydroxypropionitrile
- 65193-87-5
2-cyanoethylacetoacetate
| Conditions | Yield |
|---|---|
| With N-Bromosuccinimide In toluene at 90℃; for 3h; | 95.2% |
| With Candida antarctica lipase B at 40℃; under 10 Torr; | 88% |
| Conditions | Yield |
|---|---|
| With triethylamine In ethyl acetate at 20 - 60℃; | 86% |
| With triethylamine In ethyl acetate at 80℃; Reagent/catalyst; Large scale; | 85.8% |
| With sodium acetate for 16h; Ambient temperature; |
- 72324-39-1
5-acetyl-2,2-dimethyl-1,3-dioxane-4,6-dione
- 109-78-4
3-Hydroxypropionitrile
- 65193-87-5
2-cyanoethylacetoacetate
| Conditions | Yield |
|---|---|
| In toluene Heating; Yield given; |
- 2039-85-2
3-Chlorostyrene
- 65193-87-5
2-cyanoethylacetoacetate
- 314775-78-5
2-acetyl-3-(3-chlorophenyl)-acrylic acid (2-cyanoethyl) ester
| Conditions | Yield |
|---|---|
| piperidine; acetic acid In propanol, 2 at 20℃; | 100% |
- 13114-87-9
N-(3-trifluoromethylphenyl)urea
- 65193-87-5
2-cyanoethylacetoacetate
- 105-07-7
4-cyanobenzaldehyde
- 671776-88-8
4-(4-cyanophenyl)-6-methyl-2-oxo-1-[3-(trifluoromethyl)phenyl]-1,2,3,4-tetrahydro-pyrimidine-5-carboxylic acid 2-cyanoethyl ester
| Conditions | Yield |
|---|---|
| With ethyl phosphate In tetrahydrofuran for 18h; Heating / reflux; | 100% |
- 65193-87-5
2-cyanoethylacetoacetate
- 21731-17-9
methyl 3-aminocrotonate
- 32863-32-4
benzo[c][1,2,5]oxadiazole-4-carbaldehyde
| Conditions | Yield |
|---|---|
| In isopropyl alcohol Inert atmosphere; Reflux; | 97% |
- 21962-45-8
4-formyl-3-methoxy-benzonitrile
- 65193-87-5
2-cyanoethylacetoacetate
| Conditions | Yield |
|---|---|
| With piperidine; acetic acid In isopropyl alcohol at 0 - 30℃; for 3.5h; Solvent; Temperature; Large scale; | 97% |
| With piperidine; acetic acid In isopropyl alcohol at 0 - 30℃; for 4.5h; Solvent; Temperature; Knoevenagel Condensation; Large scale; | 97% |
| With piperidine; acetic acid In dichloromethane for 23h; Reflux; | 80.5% |
| With piperidine; acetic acid In dichloromethane Reflux; | 48% |
- 555-16-8
4-nitrobenzaldehdye
- 65193-87-5
2-cyanoethylacetoacetate
- 166809-85-4
4-(4-nitrophenyl)-3-(2-cyanoethoxy)carbonyl-3-buten-2-one
| Conditions | Yield |
|---|---|
| With piperidine; acetic acid In isopropyl alcohol for 48h; Ambient temperature; | 96% |
- 99-61-6
3-nitro-benzaldehyde
- 65193-87-5
2-cyanoethylacetoacetate
- 626-34-6, 7318-00-5, 41867-20-3
ethyl aminocrotonate
- 75130-25-5
3-(2-cyanoethyl) 5-ethyl 2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydropyridine-3,5-dicarboxylate
| Conditions | Yield |
|---|---|
| In isopropyl alcohol Inert atmosphere; Reflux; | 95% |
- Total:38 Page 1 of 1 1
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