Detail of "73960-72-2"

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Conversion of N-acetylneuraminic acid glycosyl chloride into dibenzyl glycosyl phosphate: O-glycosylation in the absence of a promoter

Conversion of N-acetylneuraminic acid glycosyl chloride into dibenzyl glycosyl phosphate: O-glycosylation in the absence of a promoter. Shpirt, A. M.; Kononov, L. O.; Torgov, V. I.; Shibaev, V. N. (N. D. 73960-72-2 and 7087-68-5 are also in the experiment. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, Moscow 119991, Russia). Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya), 53(3), 717-719 (English) 2004 Kluwer Academic/Consultants Bureau. CODEN: RCBUEY. ISSN: 1066-5285. DOCUMENT TYPE: Journal CA Section: 33 (Carbohydrates) Readily accessible N-acetylneuraminic acid (Neu5Ac) glycosyl chloride I (R = Cl), which was regarded to be a poor glycosyl donor, was shown to react with dibenzyl phosphoric acid salts in the absence of glycosylation promoters to give the corresponding b-Neu5Ac dibenzyl glycosyl phosphate I [R = OP(O)(OCH2Ph)2] in high yield. .