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880468-89-3

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Basic Information
CAS No.: 880468-89-3
Name: (R)-tert-Butyl 1-(benzylamino)-3-methoxy-1-oxopropan-2-ylcarbamate
Article Data: 26
Molecular Structure:
Molecular Structure of 880468-89-3 ((R)-tert-Butyl 1-(benzylamino)-3-methoxy-1-oxopropan-2-ylcarbamate)
Formula: C16H24 N2 O4
Molecular Weight: 308.378
Synonyms: TERT-BUTYL N-[(1R)-1-(BENZYLCARBAMOYL)-2-METHOXYETHYL]CARBAMATE;(R)-TERT-BUTYL-1-(BENZYLAMINO)-3-METHOXY-1-OXOPROPAN-2-YLCARBAMATE;(R)-N-benzyl-2-N-Boc-amino-3-methoxypropionamide;
EINECS: 1592732-453-0
Density: 1.103±0.06 g/cm3(Predicted)
Melting Point: 63-64 °C
Boiling Point: 507.6±50.0 °C(Predicted)
PSA: 76.66000
LogP: 2.62430
Related products
Synthetic route

N-Boc-O-methyl-D-serine pivalic anhydride

100-46-9

benzylamine

880468-89-3

tert-butyl [(2R)-1-(benzylamino)-3-methoxy-1-oxopropan-2-yl]carbamate

Conditions
ConditionsYield
In dichloromethane at 0 - 5℃; for 0.5h;100%
1253790-58-7

tert-butyl-N-[(1R)-2-(benzylamino)-1-(hydroxymethyl)-2-oxo-ethyl]carbamate

77-78-1

dimethyl sulfate

880468-89-3

tert-butyl [(2R)-1-(benzylamino)-3-methoxy-1-oxopropan-2-yl]carbamate

Conditions
ConditionsYield
With tetrabutylammomium bromide; sodium hydroxide In water; toluene at 0 - 30℃; for 1.5h;96.28%
With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate In dichloromethane; water at 4 - 25℃; Inert atmosphere;75.8%
Stage #1: tert-butyl-N-[(1R)-2-(benzylamino)-1-(hydroxymethyl)-2-oxo-ethyl]carbamate; dimethyl sulfate With tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide In dichloromethane; water at 4 - 25℃; Cooling with ice; Inert atmosphere;
Stage #2: With ammonium hydroxide In dichloromethane; water		75.8%

2,4-dioxo-3-azaspiro[5.5]undecan-3-yl N-(tert-butoxycarbonyl)-O-methyl-D-serinate

100-46-9

benzylamine

880468-89-3

tert-butyl [(2R)-1-(benzylamino)-3-methoxy-1-oxopropan-2-yl]carbamate

Conditions
ConditionsYield
at 20℃; for 3h;90.4%
100-46-9

benzylamine

86123-95-7

(R)-2-((tert-butoxycarbonyl)amino)-3-methoxypropionic acid

880468-89-3

tert-butyl [(2R)-1-(benzylamino)-3-methoxy-1-oxopropan-2-yl]carbamate

Conditions
ConditionsYield
Stage #1: (R)-2-((tert-butoxycarbonyl)amino)-3-methoxypropionic acid With 4-methyl-morpholine; isobutyl chloroformate In tetrahydrofuran at -78℃; Inert atmosphere;
Stage #2: benzylamine In tetrahydrofuran at -78 - 20℃; for 1h;		90%
With 4-methyl-morpholine; isobutyl chloroformate In tetrahydrofuran at -78 - 30℃; for 1h; Inert atmosphere;90%
Stage #1: (R)-2-((tert-butoxycarbonyl)amino)-3-methoxypropionic acid With 4-methyl-morpholine In tetrahydrofuran at -78℃; for 0.0833333h; Inert atmosphere;
Stage #2: benzylamine With isobutyl chloroformate In tetrahydrofuran at -78 - 20℃; for 1h; Inert atmosphere;		90%
1253790-58-7

tert-butyl-N-[(1R)-2-(benzylamino)-1-(hydroxymethyl)-2-oxo-ethyl]carbamate

420-37-1

trimethoxonium tetrafluoroborate

880468-89-3

tert-butyl [(2R)-1-(benzylamino)-3-methoxy-1-oxopropan-2-yl]carbamate

Conditions
ConditionsYield
With N,N,N',N'-tetramethyl-1,8-diaminonaphthalene In dichloromethane at 20℃; for 16h; Inert atmosphere; Green chemistry;81%
1253790-58-7

tert-butyl-N-[(1R)-2-(benzylamino)-1-(hydroxymethyl)-2-oxo-ethyl]carbamate

80-48-8

methyl p-toluene sulfonate

880468-89-3

tert-butyl [(2R)-1-(benzylamino)-3-methoxy-1-oxopropan-2-yl]carbamate

Conditions
ConditionsYield
With tetrabutylammomium bromide; potassium hydroxide In toluene at -1 - 2℃; Solvent; Reagent/catalyst; Temperature;80%
With tetrabutylammomium bromide; potassium hydroxide In water; toluene at 20℃; for 3h; Reagent/catalyst;60.97g
With tetrabutylammomium bromide; sodium hydroxide In water at 20℃; for 3h;38.5 g
With tetrabutylammomium bromide; sodium hydroxide In water; toluene at 20℃; for 3h;38.5 g
100-46-9

benzylamine

880468-89-3

tert-butyl [(2R)-1-(benzylamino)-3-methoxy-1-oxopropan-2-yl]carbamate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: 4-methyl-morpholine; isobutyl chloroformate / dichloromethane / -5 °C
1.2: -5 - 0 °C
2.1: potassium hydroxide / dichloromethane / 5 °C
2.2: 5 °C
View Scheme
Multi-step reaction with 2 steps
1.1: methyl chloroformate; 4-methyl-morpholine / dichloromethane / 0.5 h / 35 °C
1.2: 20 °C
2.1: sodium hydroxide; tetrabutylammomium bromide / toluene; water / 2 - 27 °C
View Scheme
Multi-step reaction with 2 steps
1.1: isobutyl chloroformate; 4-methyl-morpholine / dichloromethane / 5 °C
1.2: 0 - 5 °C
2.1: potassium hydroxide / 5 °C
2.2: 5 °C
View Scheme
24424-99-5

di-tert-butyl dicarbonate

880468-89-3

tert-butyl [(2R)-1-(benzylamino)-3-methoxy-1-oxopropan-2-yl]carbamate

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: sodium hydroxide / water / 10 h / 20 - 25 °C
2.1: sodium hydroxide / water / 0.5 h / 0 - 5 °C
2.2: 14 h / 5 - 10 °C
2.3: 0 - 5 °C
3.1: chloroformic acid ethyl ester; 4-methyl-morpholine / dichloromethane / 0.25 h / -15 - -10 °C
3.2: 3 h / -15 - 25 °C
View Scheme
Multi-step reaction with 3 steps
1.1: sodium hydroxide / water
1.2: 16 h / 20 °C
1.3: pH 3.5 - 4
2.1: 4-methyl-morpholine; isobutyl chloroformate / dichloromethane / 1 h / -20 - 20 °C
3.1: sodium hydroxide / tetrabutylammomium bromide / dichloromethane; water / 2 h / 5 - 20 °C
View Scheme
Multi-step reaction with 3 steps
1.1: dmap; sodium hydroxide / water; tert-butyl alcohol / 11 h / 20 °C
2.1: sodium hydroxide; tetrabutylammomium bromide / dichloromethane / 0.5 h / 0 - 5 °C
2.2: 20 °C
3.1: 4-methyl-morpholine; isobutyl chloroformate / dichloromethane / -10 - -5 °C
3.2: 20 °C
View Scheme
3262-72-4, 3850-40-6, 6368-20-3, 90582-28-8, 84311-18-2

(R)-N-tert-butoxycarbonyl serine

880468-89-3

tert-butyl [(2R)-1-(benzylamino)-3-methoxy-1-oxopropan-2-yl]carbamate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: sodium hydroxide / water / 0.5 h / 0 - 5 °C
1.2: 14 h / 5 - 10 °C
1.3: 0 - 5 °C
2.1: chloroformic acid ethyl ester; 4-methyl-morpholine / dichloromethane / 0.25 h / -15 - -10 °C
2.2: 3 h / -15 - 25 °C
View Scheme
Multi-step reaction with 2 steps
1.1: 4-methyl-morpholine; isobutyl chloroformate / dichloromethane / -5 °C
1.2: -5 - 0 °C
2.1: potassium hydroxide / dichloromethane / 5 °C
2.2: 5 °C
View Scheme
Multi-step reaction with 2 steps
1: 4-methyl-morpholine; isobutyl chloroformate / dichloromethane / 1 h / -20 - 20 °C
2: sodium hydroxide / tetrabutylammomium bromide / dichloromethane; water / 2 h / 5 - 20 °C
View Scheme

tert-butyl [(2R)-1-hydroxy-3-methoxypropan-2-yl]carbamate

880468-89-3

tert-butyl [(2R)-1-(benzylamino)-3-methoxy-1-oxopropan-2-yl]carbamate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: sodium chlorite; sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / acetonitrile / 6 h / 35 °C / pH 6.7 / aq. phosphate buffer
2.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / -78 °C / Inert atmosphere
2.2: 1 h / -78 - 20 °C
View Scheme
Multi-step reaction with 2 steps
1: sodium chlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hypochlorite / acetonitrile; aq. phosphate buffer / 7 h / 35 °C / pH 6.7
2: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 1 h / -78 - 30 °C / Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1.1: potassium dihydrogenphosphate; sodium chlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hypochlorite / acetonitrile / 3 h / 20 °C
2.1: 4-methyl-morpholine / tetrahydrofuran / 0.08 h / -78 °C / Inert atmosphere
2.2: 1 h / -78 - 20 °C / Inert atmosphere
View Scheme
Raw Materials
86123-95-7
24424-99-5
77-78-1
100-46-9
3262-72-4
3850-40-6
Downstream Products
196601-69-1
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    (R)-tert-Butyl 1-(benzylamino)-3-methoxy-1-oxopropan-2-ylcarbamate

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    880468-89-3

    Factory Supply (R)-tert-Butyl 1-(benzylamino)-3-methoxy-1-oxopropan-2-ylcar...

    Min.Order: 0 Metric Ton

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     China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:0513-87616220

    Address:Fine chemical industry park, Nantong,Jiangsu

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  • (R)-tert-Butyl 1-(benzylamino)-3-methoxy-1-oxopropan-2-ylcarbamate

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    Address:Floor 4, Building 5, No.588 Tianxiong Road, Zhoupu International Medical Zone, ShangHai, China

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

    Founded in 2008, East Chemsources Limited is a professional manufacturer of supplier in food and beverage, pharmaceuticals, cosmetics and other industries. pharmaceutical field in

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

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    Address:No.1581-12,Jinshui Road, Licang, Qingdao,China

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    Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

    Welcome to Taizhou Zhenyu Biotech Co.,LTD , Sister Company of Ningbo Zhenlei Chemical co.,ltd ,is a rapid growing company , We are one of TOP supplier and manufactuer of Human APIs

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    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    Address:Room 623 Yulan Square Bussiness Building . Jiaojiang Taizhou Zhejiang 318000 China

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    Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

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    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    (R) -2-tert-butoxycarbonyl amino-N-benzyl-3-methoxypropylamide

    Min.Order: 1 Metric Ton

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    1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

    KAISA GROUP INC.is the enterprise which is specialize in manfacturing and exporting avariety of Chemical in China. We have the strong economic base and comprehensive technology.We

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    United States  |  Contact Details

    Business Type:Trading Company

    Tel:15131197030

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    (R)-tert-Butyl 1-(benzylamino)-3-methoxy-1-oxopropan-2-ylcarbamate

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    Product Name: (R)-tert-Butyl 1-(benzylamino)-3-methoxy-1-oxopropan-2-ylcarbamate Synonyms: (R)-tert-Butyl 1-(benzylamino)-3-methoxy-1-oxopropan-2-ylc…Appearance:Solid powder Storage:Sealed,light and oxygen resistant Package:aluminum foil bag,carton

    Kono Chem Co.,Ltd is a leading producer of standardized herbal extracts, natural active ingredients and APIs for pharmaceutical, health food and cosmetic industries. Annually, mo

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     China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:86-29-86107037-8015

    Address:No.11 Daqing Road,Lianhu District,Xi’an 710082,China

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    SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-86818502

    Address:5Fl. 501Room, Tower A, New Youth Plaza, 8 Jia Shan Road, Hangzhou, China

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    (R)-tert-Butyl 1-(benzylamino)-3-methoxy-1-oxopropan-2-ylcarbamate

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    High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

    Suzhou Health Chemicals Co., Ltd. is A Fine Chemicals Company, specializing in research, development, manufacture and distribute raw materials for pharmaceutical, healthcare, bioch

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-512-58277800

    Address:No. 338, Jingang Avenue,

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  • Casno:

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    tert-butyl (R)-(1-(benzylamino)-3-methoxy-1-oxopropan-2-yl)carbamate

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    GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation

    GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production. Currently our major business is: 1.Con

  •  Golden Pharma Co., Limited

    China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:18958062155

    Address:1

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  • (R) -2-tert-butoxycarbonyl amino-N-benzyl-3-methoxypropylamide

  • Casno:

    880468-89-3

    (R) -2-tert-butoxycarbonyl amino-N-benzyl-3-methoxypropylamide

    Min.Order: 1 Metric Ton

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    We are a Union of chemistry in China, consists of chemists，engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

    We are a Union of chemistry in China, consists of chemists，engineers, laboratories,factories in China. We organize surplus capacity of R&D and production in China for chemicals cus

  •  Bluecrystal chem-union

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-1895157

    Address:Liang Xi Qu

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