6276-11-5Relevant articles and documents
Efficient synthesis of methyl carbamate via Hofmann rearrangement in the presence of TsNBr2
Borah, Arun Jyoti,Phukan, Prodeep
experimental part, p. 3035 - 3037 (2012/07/27)
An efficient method has been developed for the synthesis of carbamates from the corresponding amides via the Hofmann rearrangement using N,N-dibromo-p-toluenesulfonamide (TsNBr2) in the presence of DBU in methanol. The reaction goes into completion in 10-20 min at 65 °C to produce the corresponding carbamate in excellent yield.
METHOD FOR OPTICAL RESOLUTION OF ALKYLPIPERIDIN-3-YL CARBAMATE AND INTERMEDIATE THEREFOR
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Page/Page column 11, (2010/11/19)
Disclosed is a method for optical resolution of an alkylpiperidin-3-yl carbamate, the method including bringing an RS mixture of an alkylpiperidin-3-yl carbamate into contact with an optically active tartaric acid in the presence of a solvent.
A New and Facile Synthesis of Alkyl N-Arylcarbamates
Leardini, Rino,Zanardi, Giuseppe
, p. 225 - 227 (2007/10/02)
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