Synthesis of per-deuterated alkyl amines for the preparation of deuterated organic pyromellitamide gelators
A general, direct and scalable synthesis of per-deuterated alkyl amines is reported, together with their incorporation into pyromellitamides, which form self-assembled gels in cyclohexane. The deuterium labelling of these gelators allows the study of the dynamic intermolecular interactions in these materials using solid-state 2H NMR spectroscopy.
Yepuri, Nageshwar R.,Jamieson, Scott A.,Darwish, Tamim A.,Rawal, Aditya,Hook, James M.,Thordarson, Pall,Holden, Peter J.,James, Michael
supporting information
p. 2538 - 2541
(2013/06/27)
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