Butyric--d4 Acid

Base Information

• Chemical Name: Butyric--d4 Acid
• CAS No.: 1219794-99-6
• Molecular Formula: CH3CD2CD2COOH
• Molecular Weight: 92.13
• Mol file: 1219794-99-6.mol

Synonyms:

Chemical Property of Butyric--d4 Acid

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

Butyric-2,2,3,3-d4Acid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Butyric--d4 Acid

There total 1 articles about Butyric--d4 Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

butyric acid (107-92-6) → 4,4,4,3,3,2,2-d7-butanoic acid (156779-02-1,1219794-99-6,73607-83-7)

Guidance literature:

With [D]-sodium hydroxide; 10% Pt/activated carbon; water-d2; at 220 ℃;

DOI:10.1016/j.tetlet.2013.03.031

Reference yield:

benzoyl chloride (98-88-4) + 4,4,4,3,3,2,2-d7-butanoic acid (156779-02-1,1219794-99-6,73607-83-7) → C11H5(2)H7O3

Guidance literature:

With N,N-dimethyl-formamide; Heating;

DOI:10.1016/j.tetlet.2013.03.031

Reference yield:

4,4,4,3,3,2,2-d7-butanoic acid (156779-02-1,1219794-99-6,73607-83-7) → butyryl chloride-d7 (1219805-71-6)

Guidance literature:

With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 0 - 20 ℃; for 3h; Inert atmosphere;

DOI:10.1246/cl.150615

upstream raw materials:

butyric acid

Downstream raw materials:

<2,2,3,3,4,4,4-(2)H7>butan-1-ol

butyryl chloride-d7

Refernces