cas 122647-32-9, Ibutilide fumarate | Articles data ｜lookchem

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122647-32-9

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A novel synthesis of ibutilide fumarate
A novel protocol for the synthesis of Ibutilide Fumarate (raceme) was achieved from 2-pyrrolidinone with an overall yield of 15%. The core structure was constructed in one step based on Friedel-Crafts acylation with an acyl chloride containing an amino hydrochloride.
Wang, Tao,Tian, Rui,Xiao, Bin,Shen, Yi,Zhou, Hui,Li, Qingeng
p. 423 - 426
(2011)
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Chemical Properties

Melting Point: 112-117?C
Boiling Point: 522.4 °C at 760 mmHg
Flash Point:269.7 °C
Solubility:H2O: >20mg/mL
Storage Temp.:Refrigerator
Vapor Pressure: 9.71E-12mmHg at 25°C
Merck: 14,4883
PSA: 230.64000
LogP: 10.34740

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