cas 201227-38-5, 5-BROMO-1H-INDAZOLE-3-CARBALDEHYDE | Articles data ｜lookchem

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201227-38-5

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An optimized procedure for direct access to 1: H -indazole-3-carboxaldehyde derivatives by nitrosation of indoles
Indazole derivatives are currently drawing more and more attention in medicinal chemistry as kinase inhibitors. 1H-indazole-3-carboxaldehydes are key intermediates to access to a variety of polyfunctionalized 3-substituted indazoles. We report here a general access to this motif, based on the nitrosation of indoles in a slightly acidic environment. These very mild conditions allow the conversion of both electron-rich and electron-deficient indoles into 1H-indazole-3-carboxaldehydes.
Chevalier, Arnaud,Ouahrouch, Abdelaaziz,Arnaud, Alexandre,Gallavardin, Thibault,Franck, Xavier
p. 13121 - 13128
(2018/04/23)

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Chemical Properties

Boiling Point: 414.059 °C at 760 mmHg
Flash Point:204.216 °C
Density: 1.83 g/cm³
Storage Temp.:under inert gas (nitrogen or Argon) at 2-8°C
Vapor Pressure: 0mmHg at 25°C
Refractive Index: 1.769
PKA: 10.78±0.40(Predicted)
PSA: 45.75000
LogP: 2.13790

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