cas 2023-48-5, Triphenylbismuth Difluoride | Articles data ｜lookchem

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2023-48-5

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The use of hexafluoropropene oxide in substitutive fluorination of Sbv and Biv oxygen-containing compounds
Reactions of hexafluoropropene oxide with SbV and BiV oxygen-containing compounds were studied. The E=O (E-O) groups were found to be transformed into the EF2 (E-F) (E = Sb or Bi) groups.
Lermontov,Rakov,Zefirov
p. 1609 - 1611
(1998)
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Synthesis and structure of triphenylbismuth difluoride
The reaction of triphenylbismuth dichloride with sodium fluoride in acetone leads to formation of triphenylbismuth difluoride in 73% yield. The X-ray diffraction data show that the bismuth atom in the two symmetrically independent molecules of bismuth dif
Sharutin,Sharutina,Egorova,Ivanenko,Bel'skii
p. 44 - 45
(2007/10/03)

Reactions of triarylbismuth bis(arenesulfonates)
Reactions of triphenylbismuth with sodium salts, acids, alkalies, and zinc are studied. In the first three cases Bi-O bond cleavage takes place, while zinc reduces the starting bismuth compounds to triphenylbismuth.
Sharutin,Sharutina,Egorova,Ettenko
p. 1236 - 1237
(2007/10/03)

Unexpected Formation of Triarylbismuth Diformates in the Oxidation of Triarylbismuthines with Ozone at Low Temperatures
Oxidation of triphenylbismuthine 1 with ozone in toluene at -78 deg C gave, unexpectedly, a high yield of triphenylbismuth diformate 3, which was also obtainable as a minor product by a similar oxidation in ethyl acetate and acetone.An X-ray crystallographic study revealed that compound 3 has C2 symmetry, the geometry around the bismuth atom being best described as a distorted trigonal bipyramid as a result of strong intramolecular interaction between the bismuth and carbonyl oxygen atoms.Treatment of compound 3 with aqueous sodium acetate or halides readily converted it into the corresponding triphenylbismuth diacetate 5 or dihalides 7 - 9.
Suzuki, Hitomi,Ikegami, Tohru,Matano, Yoshihiro,Azuma, Nagao
p. 2411 - 2416
(2007/10/02)

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Chemical Properties

Melting Point: 159°C(lit.)
PSA: 0.00000
LogP: -1.19410

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