cas 2106-05-0, 5-Chloro-2-fluoroaniline | Articles data ｜lookchem

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2106-05-0

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Anion ligand promoted selective C-F bond reductive elimination enables C(sp2)-H fluorination
A detailed mechanism study on the anion ligand promoted selective C-H bond fluorination is reported. The role of the anion ligand has been clarified by experimental evidence and DFT calculations. Moreover, the nitrate promoted C-F bond reductive elimination enabled a selective C-H bond fluorination of various symmetric and asymmetric azobenzenes to access diverse o-fluoroanilines.
Mao, Yang-Jie,Luo, Gen,Hao, Hong-Yan,Xu, Zhen-Yuan,Lou, Shao-Jie,Xu, Dan-Qian
supporting information
p. 14458 - 14461
(2019/12/09)

Selective reduction of halogenated nitroarenes with hydrazine hydrate in the presence of Pd/C
A large variety of halogenated nitroarenes have been selectively reduced with hydrazine hydrate in the presence of Pd/C to give the corresponding (halogenated) anilines in good yield.
Li, Fang,Frett, Brendan,Li, Hong-Yu
p. 1403 - 1408
(2014/06/23)

SYNTHESIS OF 2-HALO-4,5-DIFLUOROBENZOIC ACIDS
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Braish, Tamim F.,Fox, Darrell E.
p. 655 - 658
(2007/10/03)

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Chemical Properties

Appearance/Colour :COLORLESS TO BROWN LIQUID
Boiling Point: 214.4 °C at 760 mmHg
Flash Point:83.5 °C
Density: 1.349 g/cm³
Storage Temp.:Keep in dark place,Inert atmosphere,Room temperature
Vapor Pressure: 0.0567mmHg at 25°C
Refractive Index: n20/D 1.561(lit.)
PKA: 2.15±0.10(Predicted)
PSA: 26.02000
LogP: 2.64250

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