Process for the preparation of 2,4-dinitro-2,4-diazapentane
The invention is a process for reacting methylnitramine with formaldehyde a halogenated solvent and reacting the methylnitramine with formaldehyde in the presence of a strong sulfuric acid catalyst at certain specific temperatures to yield a final product having a yield rate of 70% or greater dimethylmethylenedinitraamine.
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(2008/06/13)
Synthesis of dimethylmethylene dinitramine
A process for preparing 2,4-dinitro-2,4-diazapentane by (1) nitrating dimethylurea to form dimethyldinitrourea; (2) hydrolyzing the dimethyldinitrourea to form methylnitramine; (3) reacting one mole of methylamine with one mole of formaldehyde in aqus solution to form 2-nitro-2-aza-1-propanol; and (4) reaction one mole of methylnitramine with each mole of 2-nitro-2-aza-1-propanol to form one mole of 2,4-dinitro-2,4-diazapentane.
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(2008/06/13)
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