cas 3569-99-1, 3-Pyridinecarboxylic acid N-hydroxymethylamide | Articles data ｜lookchem

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3569-99-1

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3D, 2D and 1D networks via N-H... O and N-H... N hydrogen bonding by the bis-amide analogues: Effect of chain lengths and odd-even spacers
The synthesis, crystal structures and hydrogen bonding networks of four members of the bis(pyridinecarboxamido)alkane and bis(pyridyl)alkanediamides series (1 ≈ n ; 8), where the amide moieties are separated by alkyl chain (-(CH2)n-) having even or odd number of -(CH2)-groups are explored and correlated with the previously reported structures. The odd members (n = odd) of both the series are found to adopt three-dimensional networks in contrast to the 1D or 2D structures of the even members (n = even). This odd-even effect on the dimensionality of the networks however disappears with increase in chain length.
Mukherjee, Gargi,Biradha, Kumar
p. 1285 - 1290
(2014)
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Veksler et al.
(1970)
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Synthesis, characterization and biological activity of 1,3,4-substituted 2-azetidinones
Amido/imido alcohol/2-phenyl-3-hydroxyethylquinazolin-4 (3H) -one 1 on treatment with benzoic acid in the presence of cone. H2SO4 yields m-(aralkylamido/imidoalkyl/2-phenyl-3-ethyl-3H-4-oxoquinazolinyl) benzoic acids 2. The acid chloride of 2 on reaction with hydrazine hydrate affords m-(aralkylamido/imidoalkyl/2-phenyl-3-ethyl-3H-4-oxo-quinazolinyl) benzoic acid hydrazides 4 which on condensation with an aromatic aldehyde in acetic acid gives m-(aralkylamido/imidoalkyl/2-phenyl-3-ethyl-3H-4-oxo- quinazolinyl) benzoic acid hydrazones 5. Compounds 5 undergo cyclization with phenoxy acetic acid in the presence of thionyl chloride in dry benzene to furnish 1-[m-(aralkylamido/imidoalkyl/2-phenyl-3-ethyl-3H-4-oxo-quinazolinyl- benzamido)]-3-phenoxy-4-phenyl-2-azetidinones 6. The antiviral and antifungal activities of 6 have been reported.
Pandey,Gupta,Upadhyay, Mrinalini,Upadhyay, Mridula,Singh,Tandon, Meenal
p. 158 - 162
(2007/10/03)

Synthesis of nicotinic acid and hydroxymethylamide by the hydroformylation of 3-cyanopyridine
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Dzhumakaev,Makhmetov,Mai
p. 189 - 190
(2007/10/02)

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N-(2-Phenylamino-naphthalen-1-ylmethyl)-nicotinamide

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N-{3-[1-Phenyl-meth-(E)-ylidene-hydrazinocarbonyl]-benzyl}-nicotinamide

Chemical Properties

Appearance/Colour :White Solid

Melting Point: 152-154 °C(lit.)

Boiling Point: 427.7 °C at 760 mmHg

Flash Point:212.5 °C

Density: 1.262 g/cm³

Solubility:DMSO, Methanol

Storage Temp.:-20?C Freezer

Vapor Pressure: 4.46E-08mmHg at 25°C

Refractive Index: 1.569

PKA: 12.22±0.46(Predicted)

Merck: 14,4833

PSA: 62.22000

LogP: 0.15210

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