cas 3743-07-5, DIMETHYLCHLOROPHOSPHITE | Articles data ｜lookchem

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3743-07-5

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A Mechanistic Investigation of the Todd Reaction
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Kong, Anne,Engel, Robert
p. 3671 - 3672
(1985)
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THE PREPARATION OF DIMETHYL PHOSPHOROCHLORIDITE AND ITS HOMOLOGS FROM TRIALKYL PHOSPHITES AND DICHLOROTRIPHENYLPHOSPHORANE
A novel convenient sythesis of dialkyl phosphorochloridites based on the reaction of trialkyl phosphites with dichlorotriphenylphosphorane has been described.In this way the commomly used dialkyl phosphorochloridites (3a-e) were prepared in satisfactory yields.Their identity was confirmed by 31P-NMR spectroscopy as well as by their refractive index.
Majewski, Piotr
p. 37 - 40
(2007/10/02)

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Chemical Properties

Boiling Point: 96°Cat760mmHg
Flash Point:11.8°C
Density: g/cm³
Vapor Pressure: 50.8mmHg at 25°C
PSA: 32.05000
LogP: 1.74490

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