cas 53663-39-1, 2-Bromo-3-methylbenzoic acid | Articles data ｜lookchem

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53663-39-1

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METHOD FOR PRODUCING TETRAZOLINONE COMPOUND
A tetrazolinone compound represented by formula (1): [in the formula, R1 represents an alkyl group having 1-6 carbon atoms or the like] can be produced by reacting a compound represented by formula (2): [in the formula, X1 represents
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Paragraph 0142; 0143

(2017/03/21)

Halogen-metal exchange of 3-substituted 1,2-dibromoarenes: The use of long-range JCH coupling constants to determine regiochemistry
Regioselective halogen/metal exchange reactions were carried out on a series of 3-substituted-1,2-dibromoarenes. Product mixtures were quenched with CO2 to form the corresponding benzoic acid analogs to facilitate HPLC and NMR analysis. Substitution at the 3-position could readily be assigned on the basis of 2D HMBC long-range correlations, while assignment at the 2-position was not as straightforward. The use of three-bond JCH coupling constant measurements, extracted from 1-D 1H coupled 13C experiments, were necessary to render unequivocal regio assignments. Copyright
DiMichele, Lisa,Menzel, Karsten,Mills, Paul,Frantz, Doug,Nelson, Todd
p. 1041 - 1043
(2008/02/05)

Selective Oxidation of 2-Bromo-m-xylene to 2-Bromo-3-methylbenzoic Acid or 2-Bromoisophthalic Acid
Aqueous sodium dichromate oxidation of 2-bromo-m-xylene (1) under a carbon dioxide pressure gave 2-bromoisophthalic acid (58percent), while NBS-bromination of 1 followed by Sommelet oxidation to aldehyde and then potassium permanganate oxidation enabled t
Miyano, Sotaro,Fukushima, Hiroshi,Inagawa, Hideho,Hashimoto, Harukichi
p. 3285 - 3286
(2007/10/02)

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Chemical Properties

Appearance/Colour :Off-white powder
Melting Point: 135-138 ºC
Boiling Point: 308.3°Cat760mmHg
Flash Point:140.2°C
Density: 1.599g/cm³
Solubility:soluble in Methanol
Storage Temp.:Sealed in dry,Room Temperature
Vapor Pressure: 0.000297mmHg at 25°C
PKA: 2.92±0.10(Predicted)
PSA: 37.30000
LogP: 2.45570

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