cas 5600-62-4, 4-(4-Nitrophenyl)butyric acid | Articles data ｜lookchem

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5600-62-4

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Experiments on the Chaperon effect in the nitration of aromatics
A nitro group may be effectively delivered to the ortho position of alkylbenzenes, provided that a suitable chaperon function is located in α- position and a dilute of HNO3 in CH2Cl2 is used. The carbonyl function of an aldehyde or ketone is the best choice, but a carboxyl, alkoxycarbonyl, and amide groups all work well. The ether function showed a less pronounced ortho orientation effect, whereas the hydroxyl group was too prone to oxidation. Side reactions were minimal under the conditions employed. A para chaperon effect was seemingly at work in the CH2Cl2 nitration of benzenepropanenitrile. All the results were compared with the corresponding classical nitration in H2SO4.
Strazzolini, Paolo,Giumanini, Angelo G.,Runcio, Antonio,Scuccato, Massimo
p. 952 - 958
(2007/10/03)

A Mild Oxidation of Aromatic Amines
Several primary aromatic amines have been converted to the corresponding nitro compounds in good yields.The oxidant was oxone (potassium peroxymonosulfate) and the reactions were performed in 5 to 20percent aqueous acetone and buffered with sodium bicarbonate.
Webb, Kevin S.,Seneviratne, Viran
p. 2377 - 2378
(2007/10/02)

1-Aryl-3-(2-chloroethyl) ureas: Synthesis and in vitro assay as potential anticancer agents
1-Aryl-3-(2-chlorethyl) ureas and 1-aryl-3-nitrose-3-(2-chloroethyl) ureas, derived from 4-phenylbutyric acid and alkylanillines, were synthesized and their cytotoxicity was evaluated on human adenocarcinoma cells in vitro. Methyl 4-[p-[3-(2-chloroethyl)ureido]-phenyl]butyrate, 4-methyl [3-(2-chloroethyl)ureido]benzene, and 4-butyl[3-(2-chloroethyl)ureido]benzene were found to be at least as cytotoxic as 4-[p-[bis-(2-chloroethyl)amino]phenyl]butyric acid (chlorambucil), while their N-nitrose derivatives were inactive.
Gaudreault,lacroix,Page,Joly
p. 185 - 187
(2007/10/02)

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Chemical Properties

Appearance/Colour :slightly yellow
Melting Point: 90-93 °C(lit.)
Boiling Point: 393.8 °C at 760 mmHg
Flash Point:172.3 °C
Density: 1.293 g/cm³
Storage Temp.:Sealed in dry,Room Temperature
Vapor Pressure: 6.59E-07mmHg at 25°C
PKA: 4.68±0.10(Predicted)
BRN: 2051992
PSA: 83.12000
LogP: 2.52530

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