cas 60385-06-0, 4-METHOXY-2-METHYLPHENYL ISOCYANATE | Articles data ｜lookchem

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60385-06-0

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Palladium(0)-catalyzed carbon-Hydrogen bond functionalization for the synthesis of indoloquinazolinones
The indoloquinazolinone ring system has attracted considerable attention as a pharmacophore, because it shows various biological activities. The reported synthetic methods for the compound are simple and direct, but are not effective for the direct synthesis of indoloquinazolinone with a methylene group at the C-6 position. A palladium(0)-catalyzed cyclization of chloroquinazolinone via C-H functionalization was developed for a concise synthesis of indoloquinazolinone derivatives. The presence of a substituent at the C-6 position is important for obtaining the product in good yield. The conformation of the reaction intermediate, in particular the N-C-Pd bond angle, is important for the regioselectivity of the reaction.
Tsukano, Chihiro,Okuno, Masataka,Nishiguchi, Hiromi,Takemoto, Yoshiji
supporting information
p. 1533 - 1538
(2014/06/09)

Fungicidal meta-substituted strobilurin analogs
Strobilurin analogs in which the side chain is in a meta-relationship to the pharmacophore are active fungicides provided an ortho-group is also present. Syntheses, fungicidal screening results and structure-activity relationships for these compounds are described. A new pharmacophore synthesis from aniline precursors is also detailed.
Walker, Michael P.,Stevenson, Thomas M.
p. 675 - 679
(2007/10/03)

Diiodosilane: A Reagent for Mild, Efficient Conversion of Carbamates to Ureas via Isocyanates
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Gastaldi, Stephane,Weinreb, Steven M.,Stien, Didier
p. 3239 - 3240
(2007/10/03)

Neue Methode zur Synthese von Isocyanaten unter milden Bedingungen
Keywords: Arendiyldiisocyanate; Di-tert-butyldicarbonat; 4-Dimethylaminopyridin; Isocyanate
Knoelker, Hans-Joachim,Braxmeier, Tobias,Schlechtingen, Georg
p. 2746 - 2749
(2007/10/03)

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Chemical Properties

Boiling Point: 76 °C1 mm Hg(lit.)
Flash Point:>230 °F
Density: 1.121 g/mL at 25 °C(lit.)
Storage Temp.:Refrigerator (+4°C)
Vapor Pressure: 0.019mmHg at 25°C
Refractive Index: n20/D 1.546(lit.)
Sensitive: Moisture Sensitive
BRN: 7115803
PSA: 38.66000
LogP: 1.97090

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