cas 62777-90-6, 5,6ALPHA-DIHYDRO PGI2 | Articles data

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Synthesis of (+/-)-6β-Prostaglandin I1 and (+/-)-6β-Decarboxyprostaglandin I1
The known hydroxy-aldehyde (5) has been converted into 6β-decarboxyprostaglandin I1 (19) and 6β-prostaglandin I1 (3) by (i) reaction with an appropriate organometallic reagent, (ii) cyclisation via the intermediate formation of an iodonium ion, and (iii) hydrodeiodination and desilylation.
Finch, Mark A. W.,Roberts, Stanley M.,Newton, Roger F.
p. 1312 - 1316
(2007/10/02)

Organoselenium-based synthesis of oxygen-containing prostacyclins
The application of organoselenium-induced ring closures to the synthesis of stable, oxygen-containing prostacyclins is described. The strategy involves utilization of PGF2α methyl ester (3) as a starting material in a PhSeCl-induced cyclization
Nicolaou,Barnette,Magolda
p. 3480 - 3485
(2007/10/02)

Total Synthesis of (+/-)-6β-Prostaglandin I1
(+/-)-6β-Prostaglandin I1 (3) has been prepared from the readily available unsaturated aldehyde (6) in four steps.
Finch, Mark A. W.,Roberts, Stanley M.,Newton, Roger F.
p. 589 - 590
(2007/10/02)