cas 63352-99-8, 3,5-Dichlorophenylhydrazine hydrochloride | Articles data ｜lookchem

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63352-99-8

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Synthesis of Aryl Hydrazines via CuI/BMPO Catalyzed Cross-Coupling of Aryl Halides with Hydrazine Hydrate in Water
The N,N’-bis(2,6-dimethylphenyl)oxalamide was discovered as a powerful ligand for Cu-catalyzed cross-coupling of aryl halides with hydrazine hydrate, leading to the formation of a variety of aryl hydrazines at 80 oC in water under the assistance of K3PO4 and 4 mol% cetyltrimethylammonium bromide from aryl bromides and aryl iodides. Good to excellent yields were observed in most cases.
Kumar, Siripuram Vijay,Ma, Dawei
supporting information
p. 1003 - 1006
(2018/09/20)

Piecing together the puzzle: Understanding a mild, metal free reduction method for the large scale synthesis of hydrazines
A key intermediate for the synthesis of hydrazines via a mild, metal free reduction of diazonium salts has been isolated and characterized by X-ray analysis. The presence of this intermediate is general, as demonstrated by the preparation of a number of analogues. A discussion of the mechanism and potential benefits of such a process are also described.
Browne, Duncan L.,Baxendale, Ian R.,Ley, Steven V.
supporting information; experimental part
p. 10296 - 10303
(2012/01/04)

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Chemical Properties

Appearance/Colour :white to light yellow crystal powder
Melting Point: 208-210 °C (dec.)(lit.)
Boiling Point: 286.1 °C at 760 mmHg
Flash Point:126.8 °C
Storage Temp.:Keep in dark place,Sealed in dry,Room Temperature
Vapor Pressure: 0.0027mmHg at 25°C
BRN: 4208459
PSA: 38.05000
LogP: 3.85430

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