cas 811842-25-8, L-4'-TETRAHYDROPYRANYLGLYCINE | Articles data ｜lookchem

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811842-25-8

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SYNTHESIS METHOD FOR L-CYCLIC ALKYL AMINO ACID AND PHARMACEUTICAL COMPOSITION HAVING THEREOF
A synthesis method for L-cyclic alkyl amino acid and a pharmaceutical composition having the said amino acid are provide in the present disclosure provides. The synthesis method comprises: step A.) preparing a cyclic alkyl keto acid or a cyclic alkyl keto acid salt having Structural Formula (I) or Structural Formula (II), and step B.) mixing the cyclic alkyl keto acid or the cyclic alkyl keto acid salt with ammonium formate, a leucine dehydrogenase, a formate dehydrogenase and a coenzyme NAD+, and carrying out a reductive amination reaction to generate the L-cyclic alkyl amino acid, wherein the Structural Formula (I) is where n1≧1, m1≧0 and the M1 is H or a monovalent cation; the Structural Formula (II) is where n2≧0, m2≧0, the M2 is H or a monovalent cation, an amino acid sequence of the leucine dehydrogenase is SEQ ID No.1.
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Paragraph 0090; 0097

(2016/11/17)

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Chemical Properties

Boiling Point: 316.7 °C at 760 mmHg
Flash Point:145.3 °C
Density: 1.211 g/cm³
Storage Temp.:Keep in dark place,Inert atmosphere,Room temperature
Vapor Pressure: 8.62E-05mmHg at 25°C
Refractive Index: 1.505
PKA: 2.25±0.10(Predicted)
PSA: 72.55000
LogP: 0.52520

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